diethyl(ethane-1,2-diylbis(azanediyl))bis((2-hydroxyphenyl)methylene)bis(hydrogen phosphonate)

Base Information

Chemical Name:diethyl(ethane-1,2-diylbis(azanediyl))bis((2-hydroxyphenyl)methylene)bis(hydrogen phosphonate)
CAS No.:36032-64-1
Molecular Formula:C₂₀H₃₀N₂O₈P₂
Molecular Weight:488.414
Hs Code.:

Synonyms:diethyl(ethane-1,2-diylbis(azanediyl))bis((2-hydroxyphenyl)methylene)bis(hydrogen phosphonate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl(ethane-1,2-diylbis(azanediyl))bis((2-hydroxyphenyl)methylene)bis(hydrogen phosphonate)

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Technology Process of diethyl(ethane-1,2-diylbis(azanediyl))bis((2-hydroxyphenyl)methylene)bis(hydrogen phosphonate)

There total 2 articles about diethyl(ethane-1,2-diylbis(azanediyl))bis((2-hydroxyphenyl)methylene)bis(hydrogen phosphonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90-02-8
salicylaldehyde

: 107-15-3,85404-18-8
ethylenediamine

: 762-04-9
phosphonic acid diethyl ester

: 36032-64-1
diethyl(ethane-1,2-diylbis(azanediyl))bis((2-hydroxyphenyl)methylene)bis(hydrogen phosphonate)

Guidance literature:: salicylaldehyde; ethylenediamine; In ethanol; Reflux;

phosphonic acid diethyl ester; In ethanol; Reflux;
DOI:10.1016/j.ejmech.2012.01.038

Reference yield:

Diethyl phosphonate: 762-04-9,123-22-8
Diethyl phosphonate

: 94-93-9
N,N'-ethylenebis(salicylideneimine)

: 36032-64-1
diethyl(ethane-1,2-diylbis(azanediyl))bis((2-hydroxyphenyl)methylene)bis(hydrogen phosphonate)

Guidance literature:

Reference yield: 70.2%

: copper(II) acetate dihydrate

: 36032-64-1
diethyl(ethane-1,2-diylbis(azanediyl))bis((2-hydroxyphenyl)methylene)bis(hydrogen phosphonate)

: [Cu₂(diethyl(ethane-1,2-diylbis(azanediyl))bis((2-hydroxyphenyl)methylene)bis(hydrogen phosphonate)(-2H))2]*H₂O

Guidance literature:: In methanol; soln. of ligand and Cu salt in MeOH was stirred at room temp. for 4 h; filtered; slowly evapd. for 1 wk; filtered; washed (H2O, MeOH, Et2O); dried (vac.); elem. anal.;
DOI:10.1039/c1dt11006c