5-(3'-tert-butyldiphenylsilyloxy-propan-1'-yl)-2-(4-hydroxy-butan-1'-yl)-furan

Base Information

Chemical Name:5-(3'-tert-butyldiphenylsilyloxy-propan-1'-yl)-2-(4-hydroxy-butan-1'-yl)-furan
CAS No.:944382-52-9
Molecular Formula:C₂₇H₃₆O₃Si
Molecular Weight:436.667
Hs Code.:

Synonyms:5-(3'-tert-butyldiphenylsilyloxy-propan-1'-yl)-2-(4-hydroxy-butan-1'-yl)-furan

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Chemical Property of 5-(3'-tert-butyldiphenylsilyloxy-propan-1'-yl)-2-(4-hydroxy-butan-1'-yl)-furan

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Technology Process of 5-(3'-tert-butyldiphenylsilyloxy-propan-1'-yl)-2-(4-hydroxy-butan-1'-yl)-furan

There total 3 articles about 5-(3'-tert-butyldiphenylsilyloxy-propan-1'-yl)-2-(4-hydroxy-butan-1'-yl)-furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 944382-67-6
5-(3'-tert-butyldiphenylsilyloxy-propan-1'-yl)-2-(4-hydroxy-but-1'-en-1'-yl)-furan

: 944382-52-9
5-(3'-tert-butyldiphenylsilyloxy-propan-1'-yl)-2-(4-hydroxy-butan-1'-yl)-furan

Guidance literature:: With hydrogen; palladium (II) hydroxide on carbon; In methanol; at 20 ℃; for 6h;
DOI:10.1039/b703373g

Reference yield:

: 26908-23-6
3-furan-2-yl-propan-1-ol

: 944382-52-9
5-(3'-tert-butyldiphenylsilyloxy-propan-1'-yl)-2-(4-hydroxy-butan-1'-yl)-furan

Guidance literature:: Multi-step reaction with 4 steps

1.1: 97 percent / 4-dimethylaminopyridine; triethylamine / CH₂Cl₂ / 0 - 20 °C

2.1: t-butyllithium / pentane; tetrahydrofuran / 3 h / -78 - -20 °C

2.2: tributyltin chloride / pentane; tetrahydrofuran / 3 h / -20 - 20 °C

2.3: (bis)-triphenylphosphine palladium(II) chloride / pentane; tetrahydrofuran / 16 h / Heating

3.1: 0.21 g / pyridinium p-toluenesulphonate / methanol / 24 h / 20 °C

4.1: hydrogen / palladium (II) hydroxide on carbon / methanol / 6 h / 20 °C

With dmap; hydrogen; tert.-butyl lithium; pyridinium p-toluenesulfonate; triethylamine; palladium (II) hydroxide on carbon; In tetrahydrofuran; methanol; dichloromethane; pentane; 2.3: Stille coupling reaction;
DOI:10.1039/b703373g

Reference yield:

: 1027994-01-9
C₃₃H₄₈O₃Si₂

: 944382-52-9
5-(3'-tert-butyldiphenylsilyloxy-propan-1'-yl)-2-(4-hydroxy-butan-1'-yl)-furan

Guidance literature:: Multi-step reaction with 2 steps

1: 0.21 g / pyridinium p-toluenesulphonate / methanol / 24 h / 20 °C

2: hydrogen / palladium (II) hydroxide on carbon / methanol / 6 h / 20 °C

With hydrogen; pyridinium p-toluenesulfonate; palladium (II) hydroxide on carbon; In methanol;
DOI:10.1039/b703373g