<2-(2,4,6-Cycloheptatrien-1-yl)-1-(4-methoxyphenyl)ethyliden>-propandinitril

Base Information

Chemical Name:<2-(2,4,6-Cycloheptatrien-1-yl)-1-(4-methoxyphenyl)ethyliden>-propandinitril
CAS No.:116263-46-8
Molecular Formula:C₁₉H₁₆N₂O
Molecular Weight:288.349
Hs Code.:

Synonyms:<2-(2,4,6-Cycloheptatrien-1-yl)-1-(4-methoxyphenyl)ethyliden>-propandinitril

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Chemical Property of <2-(2,4,6-Cycloheptatrien-1-yl)-1-(4-methoxyphenyl)ethyliden>-propandinitril

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Technology Process of <2-(2,4,6-Cycloheptatrien-1-yl)-1-(4-methoxyphenyl)ethyliden>-propandinitril

There total 4 articles about <2-(2,4,6-Cycloheptatrien-1-yl)-1-(4-methoxyphenyl)ethyliden>-propandinitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 90522-51-3
2-(2,4,6-Cycloheptatrien-1-yl)-1-(4-methoxyphenyl)ethanon

: 109-77-3
malononitrile

: 116263-46-8
<2-(2,4,6-Cycloheptatrien-1-yl)-1-(4-methoxyphenyl)ethyliden>-propandinitril

Guidance literature:: With ammonium acetate; acetic acid; In benzene; for 24h; Heating;

Reference yield:

: 2972-85-2
2-(1-(4-methoxyphenyl)ethylidene)malononitrile

: 27081-10-3
tropylium tetrafluoroborate

: 116263-46-8
<2-(2,4,6-Cycloheptatrien-1-yl)-1-(4-methoxyphenyl)ethyliden>-propandinitril

Guidance literature:: With triethylamine; In dichloromethane; at -78 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jo4020326

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 116263-46-8
<2-(2,4,6-Cycloheptatrien-1-yl)-1-(4-methoxyphenyl)ethyliden>-propandinitril

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / acetic acid / methanol / 3 h / Ambient temperature

2: 96 percent / ammonium acetate/ conc. acetic acid / benzene / 24 h / Heating

With ammonium acetate; acetic acid; In methanol; benzene;