1,2-bis(methyleneoxybenzyl)-3-methylenecyclopropane

Base Information

Chemical Name:1,2-bis(methyleneoxybenzyl)-3-methylenecyclopropane
CAS No.:1388002-17-2
Molecular Formula:C₂₀H₂₂O₂
Molecular Weight:294.393
Hs Code.:

Synonyms:1,2-bis(methyleneoxybenzyl)-3-methylenecyclopropane

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Chemical Property of 1,2-bis(methyleneoxybenzyl)-3-methylenecyclopropane

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Technology Process of 1,2-bis(methyleneoxybenzyl)-3-methylenecyclopropane

There total 1 articles about 1,2-bis(methyleneoxybenzyl)-3-methylenecyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57476-07-0,57637-10-2,139891-19-3,57476-08-1
(Z)-2,3-bis(hydroxymethyl)-1-methylenecyclopropane

: 100-44-7
benzyl chloride

: 1388002-17-2
1,2-bis(methyleneoxybenzyl)-3-methylenecyclopropane

Guidance literature:: (Z)-2,3-bis(hydroxymethyl)-1-methylenecyclopropane; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 0.5h;

benzyl chloride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 15h;
DOI:10.1002/chem.201200271

Reference yield: 79.0%

: 694-32-6
1-methyl-2-imidazolidone

: 1388002-17-2
1,2-bis(methyleneoxybenzyl)-3-methylenecyclopropane

: cis-1-((2,3-bis((benzyloxy)methyl)cyclopropyl)methyl)-3-methylimidazolidin-2-one

Guidance literature:: With [(o-biphenylPCy₂)Au(NCMe)]SbF₆; In 1,4-dioxane; at 80 ℃; for 18h; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201410871

Reference yield: 64.0%

: 1388002-17-2
1,2-bis(methyleneoxybenzyl)-3-methylenecyclopropane

: 100-52-7
benzaldehyde

: 1388002-01-4
C₂₇H₃₀O₃

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; triethyl borane; tricyclohexylphosphine; In tetrahydrofuran; hexane; at 20 ℃; for 16h; stereoselective reaction;
DOI:10.1002/chem.201200271