methyl 2-(N-benzyl-2,2,2-tichloroethanamido)-3-trichloroacetoxy propanoate

Base Information

Chemical Name:methyl 2-(N-benzyl-2,2,2-tichloroethanamido)-3-trichloroacetoxy propanoate
CAS No.:283602-68-6
Molecular Formula:C₁₅H₁₃Cl₆NO₅
Molecular Weight:499.99
Hs Code.:

Synonyms:methyl 2-(N-benzyl-2,2,2-tichloroethanamido)-3-trichloroacetoxy propanoate

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Chemical Property of methyl 2-(N-benzyl-2,2,2-tichloroethanamido)-3-trichloroacetoxy propanoate

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Technology Process of methyl 2-(N-benzyl-2,2,2-tichloroethanamido)-3-trichloroacetoxy propanoate

There total 1 articles about methyl 2-(N-benzyl-2,2,2-tichloroethanamido)-3-trichloroacetoxy propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 144001-42-3
methyl 2-(benzylamino)-3-hydroxypropanoate

: 76-02-8
trifluoroacetyl chloride

: 283602-68-6
methyl 2-(N-benzyl-2,2,2-tichloroethanamido)-3-trichloroacetoxy propanoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield: 88.0%

: 283602-68-6
methyl 2-(N-benzyl-2,2,2-tichloroethanamido)-3-trichloroacetoxy propanoate

: 178100-18-0
methyl 2-(N-benzyl-2,2,2-trichloroethanamido)propenoate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; for 72h; Heating;

Reference yield:

: 283602-68-6
methyl 2-(N-benzyl-2,2,2-tichloroethanamido)-3-trichloroacetoxy propanoate

: methyl (N-benzyl-4,4-dichloro)pyroglutamate

Guidance literature:: Multi-step reaction with 2 steps

1: DBU / CH₂Cl₂ / 96 h / Heating

2: 81 percent / Bu₃SnH, AIBN / benzene / 3 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; benzene;
DOI:10.1016/0040-4020(96)00288-8