3-(4-methoxyphenyl)propioloyl chloride

Base Information

Chemical Name:3-(4-methoxyphenyl)propioloyl chloride
CAS No.:131292-14-3
Molecular Formula:C₁₀H₇ClO₂
Molecular Weight:194.617
Hs Code.:

Synonyms:3-(4-methoxyphenyl)propioloyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-methoxyphenyl)propioloyl chloride

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Technology Process of 3-(4-methoxyphenyl)propioloyl chloride

There total 9 articles about 3-(4-methoxyphenyl)propioloyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2227-57-8
3-(4-methoxyphenyl)propynoic acid

: 131292-14-3
3-(4-methoxyphenyl)propioloyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; for 12h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201900947

Reference yield:

: 7515-17-5
methyl 3-(4-methoxyphenyl)propynoate

: 131292-14-3
3-(4-methoxyphenyl)propioloyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 0.24 N aq. NaOH / ethanol / 1.5 h

2: thionyl chloride / 16 h

With sodium hydroxide; thionyl chloride; In ethanol;
DOI:10.1021/jo00392a031

Reference yield:

: 100-66-3
methoxybenzene

: 131292-14-3
3-(4-methoxyphenyl)propioloyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) AlCl₃, 3.) NaHCO₃

2: 1 N aq. HCl / CH₂Cl₂

3: 0.24 N aq. NaOH / ethanol / 1.5 h

4: thionyl chloride / 16 h

With hydrogenchloride; sodium hydroxide; aluminium trichloride; thionyl chloride; sodium hydrogencarbonate; In ethanol; dichloromethane;
DOI:10.1021/jo00392a031