2-(2-amino-3-benzoyl-phenyl)acetic acid

Base Information

• Chemical Name: 2-(2-amino-3-benzoyl-phenyl)acetic acid
• CAS No.: 61941-56-8
• Molecular Formula: C15H13 N O3 . Na
• Molecular Weight: 277.255
• Hs Code.: 2922499990

Synonyms:Benzeneaceticacid, 2-amino-3-benzoyl-, monosodium salt (9CI); AHR 5850; AHR 5850D; Amfenacsodium; Phenazox; Sodium (2-amino-3-benzoylphenyl)acetate; Sodium2-amino-3-benzoylbenzeneacetate

Chemical Property of 2-(2-amino-3-benzoyl-phenyl)acetic acid

Chemical Property:

• PSA: 83.22000
• LogP: 1.37340
• Storage Temp.: Hygroscopic, -20°C Freezer, Under inert atmosphere
• Solubility.: DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

Sodium2-(2-Amino-3-benzoylphenyl)acetate ^*data from reagent suppliers

Safty Information:

• Safety Statements: Poison by subcutaneous, intramuscular, intravenous, and intraperitoneal routes. Moderately toxic by ingestion. An experimental t

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(2-amino-3-benzoyl-phenyl)acetic acid

There total 11 articles about 2-(2-amino-3-benzoyl-phenyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

7-benzoyl-1,3-dihydroindol-2-one (51135-38-7) → 2-amino-3-benzoylbenzeneacetic acid,sodium salt (61941-56-8)

Guidance literature:

With sodium hydroxide; In ethanol; toluene; for 5h; Heating;

DOI:10.1002/jhet.5570170804

Reference yield:

7-benzoyl-3-methylsulfanyl-1,3-dihydro-indol-2-one (61085-33-4) → 2-amino-3-benzoylbenzeneacetic acid,sodium salt (61941-56-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / Raney nickel / tetrahydrofuran / 0.17 h

2: 80 percent / 3N aq. NaOH / 18 h / Heating

With sodium hydroxide; nickel; In tetrahydrofuran;

DOI:10.1021/jm00377a001

Reference yield:

(2-Amino-3-benzoyl-phenyl)-methylsulfanyl-acetic acid ethyl ester → 2-amino-3-benzoylbenzeneacetic acid,sodium salt (61941-56-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 3N aq. HCl / CH₂Cl₂ / 2 h / Heating

2: 94 percent / Raney nickel / tetrahydrofuran / 0.17 h

3: 80 percent / 3N aq. NaOH / 18 h / Heating

With hydrogenchloride; sodium hydroxide; nickel; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jm00377a001

upstream raw materials:

7-benzoyl-1,3-dihydroindol-2-one

7-benzoyl-3-methylsulfanyl-1,3-dihydro-indol-2-one

(2-aminophenyl)(phenyl)methanone

1-indoline

Downstream raw materials:

methyl 2-amino-3-benzoylphenylacetate

2-amino-3-benzoylbenzeneacetic acid,ethyl ester

2-amino-3-(hydroxyphenylmethyl)benzeneacetic acid, sodium salt

2-amino-3-(phenylmethyl)benzeneacetic acid, sodium salt

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