(4-[trifluoromethyl]phenyl) N,N-dimethylsulfamate

Base Information

Chemical Name:(4-[trifluoromethyl]phenyl) N,N-dimethylsulfamate
CAS No.:1201594-37-7
Molecular Formula:C₉H₁₀F₃NO₃S
Molecular Weight:269.245
Hs Code.:

Synonyms:(4-[trifluoromethyl]phenyl) N,N-dimethylsulfamate

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Chemical Property of (4-[trifluoromethyl]phenyl) N,N-dimethylsulfamate

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Technology Process of (4-[trifluoromethyl]phenyl) N,N-dimethylsulfamate

There total 1 articles about (4-[trifluoromethyl]phenyl) N,N-dimethylsulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 402-45-9
4-hydroxybenzotrifluoride

: 13360-57-1
dimethylamino sulfonyl chloride

: 1201594-37-7
(4-[trifluoromethyl]phenyl) N,N-dimethylsulfamate

Guidance literature:: 4-hydroxybenzotrifluoride; With sodium hydride; In 1,2-dimethoxyethane; mineral oil; at 0 - 23 ℃; for 0.166667h;

dimethylamino sulfonyl chloride; In 1,2-dimethoxyethane; mineral oil; at 23 ℃; for 11h;
DOI:10.1021/ja906477r

Reference yield: 93.0%

: 123-75-1
pyrrolidine

: 1201594-37-7
(4-[trifluoromethyl]phenyl) N,N-dimethylsulfamate

: 113845-68-4
1-(4(-trifluoromethyl)phenyl)pyrrolidine

Guidance literature:: With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; sodium t-butanolate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; In 1,4-dioxane; at 80 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.201007325

Reference yield: 93.0%

: 98437-24-2
benzofuran-2-boronic acid

: 1201594-37-7
(4-[trifluoromethyl]phenyl) N,N-dimethylsulfamate

: 2-(4’-trifluoromethylphenyl)benzofuran

Guidance literature:: With C₄₆H₆₄ClPPd; potassium carbonate; In methanol; toluene; at 20 ℃; for 4h; Inert atmosphere; Glovebox; Sealed tube;
DOI:10.1021/acs.orglett.6b02330