(4R,5S,αS)-4-[N-benzyl-N-(α-methylbenzyl)amino]-5-methyltetrahydro-2-furanone

Base Information

Chemical Name:(4R,5S,αS)-4-[N-benzyl-N-(α-methylbenzyl)amino]-5-methyltetrahydro-2-furanone
CAS No.:1003280-35-0
Molecular Formula:C₂₀H₂₃NO₂
Molecular Weight:309.408
Hs Code.:

Synonyms:(4R,5S,αS)-4-[N-benzyl-N-(α-methylbenzyl)amino]-5-methyltetrahydro-2-furanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5S,αS)-4-[N-benzyl-N-(α-methylbenzyl)amino]-5-methyltetrahydro-2-furanone

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Technology Process of (4R,5S,αS)-4-[N-benzyl-N-(α-methylbenzyl)amino]-5-methyltetrahydro-2-furanone

There total 1 articles about (4R,5S,αS)-4-[N-benzyl-N-(α-methylbenzyl)amino]-5-methyltetrahydro-2-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1003280-22-5
tert-butyl (3R,4S,αS)-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-(tert-butyldimethylsilyloxy)pentanoate

: 1003280-35-0
(4R,5S,αS)-4-[N-benzyl-N-(α-methylbenzyl)amino]-5-methyltetrahydro-2-furanone

Guidance literature:: tert-butyl (3R,4S,αS)-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-(tert-butyldimethylsilyloxy)pentanoate; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 50 ℃; for 24h;

With trifluoroacetic acid; In toluene; at 20 ℃; for 24h; Further stages.;
DOI:10.1039/b712937h

Reference yield: 64.0%

: 1003280-35-0
(4R,5S,αS)-4-[N-benzyl-N-(α-methylbenzyl)amino]-5-methyltetrahydro-2-furanone

: 64-17-5
ethanol

: 98-88-4
benzoyl chloride

: 1003280-40-7
(4R,5S)-4-(N-benzoylamino)-5-methyltetrahydro-2-furanone

: 1003280-42-9
ethyl (3R,4S)-3-(N-benzoylamino)-4-hydroxypentanoate

Guidance literature:: (4R,5S,αS)-4-[N-benzyl-N-(α-methylbenzyl)amino]-5-methyltetrahydro-2-furanone; ethanol; With hydrogen; palladium on activated charcoal; at 60 ℃; for 48h; under 4560.31 Torr;

benzoyl chloride; With pyridine; In dichloromethane; at 20 ℃; for 48h; Further stages.;
DOI:10.1039/b712937h