zinc(II) 5,15-bis-(3,5-di-tert-butylphenyl)-10-phenyl-20-bromoporphyrin

Base Information

Chemical Name:zinc(II) 5,15-bis-(3,5-di-tert-butylphenyl)-10-phenyl-20-bromoporphyrin
CAS No.:444103-21-3
Molecular Formula:C₅₄H₅₅BrN₄Zn
Molecular Weight:905.351
Hs Code.:

Synonyms:zinc(II) 5,15-bis-(3,5-di-tert-butylphenyl)-10-phenyl-20-bromoporphyrin

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Chemical Property of zinc(II) 5,15-bis-(3,5-di-tert-butylphenyl)-10-phenyl-20-bromoporphyrin

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Technology Process of zinc(II) 5,15-bis-(3,5-di-tert-butylphenyl)-10-phenyl-20-bromoporphyrin

There total 6 articles about zinc(II) 5,15-bis-(3,5-di-tert-butylphenyl)-10-phenyl-20-bromoporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 5-bromo-15-phenyl-10,20-bis(3,5-di-tert-butylphenyl)porphyrin

: 557-34-6
zinc diacetate

: 444103-21-3
C₅₄H₅₅BrN₄Zn

Guidance literature:: In methanol; dichloromethane; for 2h; Inert atmosphere; Reflux;
DOI:10.1021/ol500191j

Reference yield: 89.0%

: 5-bromo-15-phenyl-10,20-bis(3,5-di-tert-butylphenyl)porphyrin

: 444103-21-3
C₅₄H₅₅BrN₄Zn

Guidance literature:: With zinc diacetate; In methanol; chloroform; at 60 ℃; for 0.5h;
DOI:10.1002/ejoc.201100642

Reference yield:

: 5,15-bis(3',5'-di-tert-butylphenyl)porphyrin

: 444103-21-3
C₅₄H₅₅BrN₄Zn

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 1.25 h / -78 - 20 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: pyridine; N-Bromosuccinimide / chloroform

3.1: zinc diacetate / methanol; chloroform / 0.5 h / 60 °C

With pyridine; N-Bromosuccinimide; zinc diacetate; In tetrahydrofuran; methanol; chloroform;
DOI:10.1002/ejoc.201100642