rac-methyl 2-{[(benzyloxy)carbonyl]amino}-6,6,7,7,7-pentafluoroheptanoate

Base Information

Chemical Name:rac-methyl 2-{[(benzyloxy)carbonyl]amino}-6,6,7,7,7-pentafluoroheptanoate
CAS No.:1609166-22-4
Molecular Formula:C₁₆H₁₈F₅NO₄
Molecular Weight:383.315
Hs Code.:

Synonyms:rac-methyl 2-{[(benzyloxy)carbonyl]amino}-6,6,7,7,7-pentafluoroheptanoate

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Chemical Property of rac-methyl 2-{[(benzyloxy)carbonyl]amino}-6,6,7,7,7-pentafluoroheptanoate

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Technology Process of rac-methyl 2-{[(benzyloxy)carbonyl]amino}-6,6,7,7,7-pentafluoroheptanoate

There total 2 articles about rac-methyl 2-{[(benzyloxy)carbonyl]amino}-6,6,7,7,7-pentafluoroheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609166-21-3
rac-methyl 2-amino-6,6,7,7,7-pentafluoroheptanoate hydrochloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 1609166-22-4
rac-methyl 2-{[(benzyloxy)carbonyl]amino}-6,6,7,7,7-pentafluoroheptanoate

Guidance literature:: With potassium carbonate; In tetrahydrofuran; water; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 252947-01-6
1-methanesulfonyloxy-4,4,5,5,5-pentafluoropentane

: 1609166-22-4
rac-methyl 2-{[(benzyloxy)carbonyl]amino}-6,6,7,7,7-pentafluoroheptanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / 1,4-dioxane; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: 50 °C

1.3: 20 °C

2.1: potassium carbonate / tetrahydrofuran; water / 0 - 20 °C / Inert atmosphere

With potassium tert-butylate; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; water;