benzyl 2-((S)-5-cyclohexyl-2,3-dihydro-2-oxo-1H-benzo[e][1,4]diazepin-3-yl)acetate

Base Information

Chemical Name:benzyl 2-((S)-5-cyclohexyl-2,3-dihydro-2-oxo-1H-benzo[e][1,4]diazepin-3-yl)acetate
CAS No.:936827-67-7
Molecular Formula:C₂₄H₂₆N₂O₃
Molecular Weight:390.482
Hs Code.:

Synonyms:benzyl 2-((S)-5-cyclohexyl-2,3-dihydro-2-oxo-1H-benzo[e][1,4]diazepin-3-yl)acetate

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Chemical Property of benzyl 2-((S)-5-cyclohexyl-2,3-dihydro-2-oxo-1H-benzo[e][1,4]diazepin-3-yl)acetate

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Technology Process of benzyl 2-((S)-5-cyclohexyl-2,3-dihydro-2-oxo-1H-benzo[e][1,4]diazepin-3-yl)acetate

There total 4 articles about benzyl 2-((S)-5-cyclohexyl-2,3-dihydro-2-oxo-1H-benzo[e][1,4]diazepin-3-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 885514-92-1
benzyl (S)-3-((2-cyclohexylcarbonyl)phenylcarbamoyl)-3-aminopropanoate

: 936827-67-7
benzyl 2-((S)-5-cyclohexyl-2,3-dihydro-2-oxo-1H-benzo[e][1,4]diazepin-3-yl)acetate

Guidance literature:: With ammonium acetate; acetic acid; at 20 ℃; for 24h;
DOI:10.1021/jm051219x

Reference yield:

: 7536-58-5,98482-77-0
BOC-L-aspartic acid 4-benzyl ester

: 936827-67-7
benzyl 2-((S)-5-cyclohexyl-2,3-dihydro-2-oxo-1H-benzo[e][1,4]diazepin-3-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / 2-ethoxy-1-ethoxycarbonyl-1,2-dihydroquinoline / CH₂Cl₂ / 24 h / 20 °C

2: 99 percent / trifluoroacetic acid / 1 h / 20 °C

3: 77 percent / ammonium acetate; acetic acid / 24 h / 20 °C

With ammonium acetate; acetic acid; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm051219x

Reference yield:

: 3432-87-9
(2-aminophenyl)cyclohexylmethanone

: 936827-67-7
benzyl 2-((S)-5-cyclohexyl-2,3-dihydro-2-oxo-1H-benzo[e][1,4]diazepin-3-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / 2-ethoxy-1-ethoxycarbonyl-1,2-dihydroquinoline / CH₂Cl₂ / 24 h / 20 °C

2: 99 percent / trifluoroacetic acid / 1 h / 20 °C

3: 77 percent / ammonium acetate; acetic acid / 24 h / 20 °C

With ammonium acetate; acetic acid; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm051219x