C₃₇H₃₈BrN₃O₅SSi

Base Information

• Chemical Name: C₃₇H₃₈BrN₃O₅SSi
• CAS No.: 1252612-11-5
• Molecular Formula: C₃₇H₃₈BrN₃O₅SSi
• Molecular Weight: 744.781
• Mol file: 1252612-11-5.mol

Synonyms:C₃₇H₃₈BrN₃O₅SSi

Chemical Property of C₃₇H₃₈BrN₃O₅SSi

Chemical Property:

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Technology Process of C₃₇H₃₈BrN₃O₅SSi

There total 1 articles about C₃₇H₃₈BrN₃O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C36H36BrN3O5SSi (1252612-09-1) + methyl iodide (74-88-4) → C37H38BrN3O5SSi (1252612-11-5)

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; at -78 - -40 ℃; for 2.83333h; Inert atmosphere;

DOI:10.1021/ja106869s

Reference yield: 85.0%

C37H38BrN3O5SSi (1252612-11-5) + acetyl chloride (75-36-5) → C23H22BrN3O6S (1252612-13-7)

Guidance literature:

C₃₇H₃₈BrN₃O₅SSi; With pyridine hydrofluoride; In tetrahydrofuran; pyridine; for 36h; Inert atmosphere;

acetyl chloride; In tetrahydrofuran; pyridine; at 23 ℃; for 44h;

DOI:10.1021/ja106869s

upstream raw materials:

C₃₆H₃₆BrN₃O₅SSi

methyl iodide

Downstream raw materials:

C₂₃H₂₂BrN₃O₆S