2-chloro-benzoic acid (3,5-dichloro-2-hydroxy-benzylidene)-hydrazide

Base Information

• Chemical Name: 2-chloro-benzoic acid (3,5-dichloro-2-hydroxy-benzylidene)-hydrazide
• CAS No.: 316149-50-5
• Molecular Formula: C₁₄H₉Cl₃N₂O₂
• Molecular Weight: 343.597
• Mol file: 316149-50-5.mol

Synonyms:2-chloro-benzoic acid (3,5-dichloro-2-hydroxy-benzylidene)-hydrazide

Chemical Property of 2-chloro-benzoic acid (3,5-dichloro-2-hydroxy-benzylidene)-hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-chloro-benzoic acid (3,5-dichloro-2-hydroxy-benzylidene)-hydrazide

There total 2 articles about 2-chloro-benzoic acid (3,5-dichloro-2-hydroxy-benzylidene)-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-chlorobenzoylhydrazide (5814-05-1) + 3,5-dichlorosalicyclaldehyde (90-60-8) → 2-chloro-benzoic acid (3,5-dichloro-2-hydroxy-benzylidene)-hydrazide (316149-50-5)

Guidance literature:

In methanol; at 20 ℃; for 0.5h;

DOI:10.1134/S1070328419040109

Reference yield:

→ 2-chloro-benzoic acid (3,5-dichloro-2-hydroxy-benzylidene)-hydrazide (316149-50-5)

Guidance literature:

Reference yield: 84.0%

bis-triphenylphosphine-palladium(II) chloride (13965-03-2) + 2-chloro-benzoic acid (3,5-dichloro-2-hydroxy-benzylidene)-hydrazide (316149-50-5) → C32H22Cl3N2O2PPd

Guidance literature:

With triethylamine; In methanol; dichloromethane; for 6h; Reflux;

DOI:10.1016/j.ica.2020.119868

upstream raw materials:

2-chlorobenzoylhydrazide

3,5-dichlorosalicyclaldehyde