di-tert-butyl 1-(2-methanesulfonyloxy-3,5-dibromophenyl)-hydrazine-1,2-dicarboxylate

Base Information

Chemical Name:di-tert-butyl 1-(2-methanesulfonyloxy-3,5-dibromophenyl)-hydrazine-1,2-dicarboxylate
CAS No.:1338466-33-3
Molecular Formula:C₁₇H₂₄Br₂N₂O₇S
Molecular Weight:560.261
Hs Code.:

Synonyms:di-tert-butyl 1-(2-methanesulfonyloxy-3,5-dibromophenyl)-hydrazine-1,2-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-tert-butyl 1-(2-methanesulfonyloxy-3,5-dibromophenyl)-hydrazine-1,2-dicarboxylate

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Technology Process of di-tert-butyl 1-(2-methanesulfonyloxy-3,5-dibromophenyl)-hydrazine-1,2-dicarboxylate

There total 1 articles about di-tert-butyl 1-(2-methanesulfonyloxy-3,5-dibromophenyl)-hydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 119440-89-0
2,4,6-tribromophenyl methanesulfonate

: 1338466-33-3
di-tert-butyl 1-(2-methanesulfonyloxy-3,5-dibromophenyl)-hydrazine-1,2-dicarboxylate

Guidance literature:: 2,4,6-tribromophenyl methanesulfonate; With isopropylmagnesium bromide; In tetrahydrofuran; 3-methyltetrahydrofuran; at -40 ℃; for 2h; Inert atmosphere;

di-tert-butyl-diazodicarboxylate; In tetrahydrofuran; 3-methyltetrahydrofuran; at -40 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo201866c

Reference yield: 65.0%

: 40167-10-0
2-[4-(benzyloxy)phenyl]acetaldehyde

: 1338466-33-3
di-tert-butyl 1-(2-methanesulfonyloxy-3,5-dibromophenyl)-hydrazine-1,2-dicarboxylate

: 1338466-36-6
3-(4-benzyloxyphenyl)-4,6-dibromo-7-methanesulfonyloxyindole

Guidance literature:: 2-[4-(benzyloxy)phenyl]acetaldehyde; di-tert-butyl 1-(2-methanesulfonyloxy-3,5-dibromophenyl)-hydrazine-1,2-dicarboxylate; With toluene-4-sulfonic acid; In ethanol; for 1h; Inert atmosphere; Reflux;

With sodium hydrogencarbonate; In water; ethyl acetate; Saturated solution; Inert atmosphere;
DOI:10.1021/jo201866c