2,4,6-tribromophenyl methanesulfonate

Base Information

Chemical Name:2,4,6-tribromophenyl methanesulfonate
CAS No.:119440-89-0
Molecular Formula:C₇H₅Br₃O₃S
Molecular Weight:408.893
Hs Code.:

Synonyms:2,4,6-tribromophenyl methanesulfonate

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Chemical Property of 2,4,6-tribromophenyl methanesulfonate

Chemical Property:

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Technology Process of 2,4,6-tribromophenyl methanesulfonate

There total 1 articles about 2,4,6-tribromophenyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 124-63-0
methanesulfonyl chloride

: 118-79-6
2,4,6-tribromophenol

: 119440-89-0
2,4,6-tribromophenyl methanesulfonate

Guidance literature:: With pyridine; triethylamine; for 1h; Ambient temperature;

Reference yield: 98.0%

: 119440-89-0
2,4,6-tribromophenyl methanesulfonate

: 106-45-6
para-thiocresol

: 43633-03-0
methanesulfinate

: 103-19-5
di(p-tolyl) disulfide

Guidance literature:: With sodium hydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; Mechanism; Ambient temperature; the reduction of various tribromophenyl sulfonates with mercaptide anions;

Reference yield: 80.0%

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 119440-89-0
2,4,6-tribromophenyl methanesulfonate

: 1338466-33-3
di-tert-butyl 1-(2-methanesulfonyloxy-3,5-dibromophenyl)-hydrazine-1,2-dicarboxylate

Guidance literature:: 2,4,6-tribromophenyl methanesulfonate; With isopropylmagnesium bromide; In tetrahydrofuran; 3-methyltetrahydrofuran; at -40 ℃; for 2h; Inert atmosphere;

di-tert-butyl-diazodicarboxylate; In tetrahydrofuran; 3-methyltetrahydrofuran; at -40 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo201866c