9-cyclohexyl-5⁽⁷⁾-(dimethyl sulfide)-nido-decaborane⁽¹¹⁾

Base Information

Chemical Name:9-cyclohexyl-5⁽⁷⁾-(dimethyl sulfide)-nido-decaborane⁽¹¹⁾
CAS No.:72765-44-7
Molecular Formula:C₈H₂₈B₁₀S
Molecular Weight:264.486
Hs Code.:

9-cyclohexyl-5<sup>(7)</sup>-(dimethyl sulfide)-nido-decaborane<sup>(11)</sup>

Synonyms:9-cyclohexyl-5⁽⁷⁾-(dimethyl sulfide)-nido-decaborane⁽¹¹⁾

Suppliers and Price of 9-cyclohexyl-5⁽⁷⁾-(dimethyl sulfide)-nido-decaborane⁽¹¹⁾

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 9-cyclohexyl-5⁽⁷⁾-(dimethyl sulfide)-nido-decaborane⁽¹¹⁾

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 9-cyclohexyl-5⁽⁷⁾-(dimethyl sulfide)-nido-decaborane⁽¹¹⁾

There total 1 articles about 9-cyclohexyl-5⁽⁷⁾-(dimethyl sulfide)-nido-decaborane⁽¹¹⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28377-92-6
bis(dimethyl sulfide) arachno-decaborane⁽¹⁴⁾

: 110-83-8
cyclohexene

: 72765-44-7
9-cyclohexyl-5⁽⁷⁾-(dimethyl sulfide)-nido-decaborane⁽¹¹⁾

Guidance literature:: In benzene; under N2 soln. warmed at 80°C for 6 h; soln. cooled, solvents removed on rotary evaporator, residue dissolved in benzene-hexane mixt., soln. chromd., B10H11C6H11S(CH3)2 collected, solvent removed, residue recrystd. from benzene-hexane; elem. anal.;
DOI:10.1021/ic50207a014

Reference yield: 96.0%

: 72765-44-7
9-cyclohexyl-5⁽⁷⁾-(dimethyl sulfide)-nido-decaborane⁽¹¹⁾

: 75-57-0
tetramethlyammonium chloride

: tetramethylammonium nonahydro-2-cyclohexyl-closo-decaborate^(2-) sesquihydrate

Guidance literature:: With NaH; In tetrahydrofuran; water; under N2 into THF added decaborane and NaH, after heating at 90°C for 24 h soln. cooled, H2O added to it over 1 h, solvent removed on rotary evaporator, resin in H(1+) form added, soln. filtered, concd., excess N(CH3)4Cl added; salt dried, recrystd. from ethanol-water; elem. anal.;
DOI:10.1021/ic50207a014

Reference yield: 94.0%

: 110-86-1
pyridine

: 72765-44-7
9-cyclohexyl-5⁽⁷⁾-(dimethyl sulfide)-nido-decaborane⁽¹¹⁾

: 72765-41-4
6-cyclohexyl-6,9-bis(pyridine)-arachno-decaborane⁽¹¹⁾

Guidance literature:: In benzene; under N2 at room temp. for 24 h; solvent removed by filtration, crystals washed with benzene-hexane, dried in vac.; elem. anal.;
DOI:10.1021/ic50207a014