2-ethoxy-1,2,3,4-tetrahydro-1-isopropyl-3-phenyl-1,3,2-benzodiazaphosphorine

Base Information

Chemical Name:2-ethoxy-1,2,3,4-tetrahydro-1-isopropyl-3-phenyl-1,3,2-benzodiazaphosphorine
CAS No.:145429-28-3
Molecular Formula:C₁₈H₂₃N₂OP
Molecular Weight:314.367
Hs Code.:

Synonyms:2-ethoxy-1,2,3,4-tetrahydro-1-isopropyl-3-phenyl-1,3,2-benzodiazaphosphorine

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Chemical Property of 2-ethoxy-1,2,3,4-tetrahydro-1-isopropyl-3-phenyl-1,3,2-benzodiazaphosphorine

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Technology Process of 2-ethoxy-1,2,3,4-tetrahydro-1-isopropyl-3-phenyl-1,3,2-benzodiazaphosphorine

There total 2 articles about 2-ethoxy-1,2,3,4-tetrahydro-1-isopropyl-3-phenyl-1,3,2-benzodiazaphosphorine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1498-42-6
phosphorodichloridous acid ethyl ester

: 145429-25-0
o-anilino-N-isopropylbenzylamine

: 145429-28-3
2-ethoxy-1,2,3,4-tetrahydro-1-isopropyl-3-phenyl-1,3,2-benzodiazaphosphorine

Guidance literature:: With triethylamine; In benzene; for 1h; Ambient temperature;

Reference yield:

: 20877-84-3
2-aminomethyl-N-phenylaniline

: 145429-28-3
2-ethoxy-1,2,3,4-tetrahydro-1-isopropyl-3-phenyl-1,3,2-benzodiazaphosphorine

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / H₂ / PtO₂ / ethanol / 100 °C

2: 58 percent / triethylamine / benzene / 1 h / Ambient temperature

With hydrogen; triethylamine; platinum(IV) oxide; In ethanol; benzene;

Reference yield: 88.0%

: acetylacetonatodicarbonylrhodium(l)

: 145429-28-3
2-ethoxy-1,2,3,4-tetrahydro-1-isopropyl-3-phenyl-1,3,2-benzodiazaphosphorine

: acetylacetonatobis(2-ethoxy-3-isopropyl-1-phenyl-1,2,3,4-tetrahydro-1,3,2-benzodiazaphosphorin)rhodium(I)

Guidance literature:: In benzene; heating AcAcRh(CO)2 and the ligand in the ratio 1:2 in anhyd. benzene at 60°C (30 min), removing of solvent; chromy. (Silufol plates, benzene-dioxane (3:1)), recrystn. (hexane); elem. anal.;