2'-<6'-((2''S,3''S-2''-chloro-3''-methylpentanoyl)oxy)>naphthyl 4-decyloxybenzoate

Base Information

• Chemical Name: 2'-<6'-((2''S,3''S-2''-chloro-3''-methylpentanoyl)oxy)>naphthyl 4-decyloxybenzoate
• CAS No.: 143238-71-5
• Molecular Formula: C₃₃H₄₁ClO₅
• Molecular Weight: 553.139
• Mol file: 143238-71-5.mol

Synonyms:2'-<6'-((2''S,3''S-2''-chloro-3''-methylpentanoyl)oxy)>naphthyl 4-decyloxybenzoate

Chemical Property of 2'-<6'-((2''S,3''S-2''-chloro-3''-methylpentanoyl)oxy)>naphthyl 4-decyloxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2'-<6'-((2''S,3''S-2''-chloro-3''-methylpentanoyl)oxy)>naphthyl 4-decyloxybenzoate

There total 5 articles about 2'-<6'-((2''S,3''S-2''-chloro-3''-methylpentanoyl)oxy)>naphthyl 4-decyloxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2.6-dihydroxynaphthalene (581-43-1) → 2'-<6'-((2''S,3''S-2''-chloro-3''-methylpentanoyl)oxy)>naphthyl 4-decyloxybenzoate (143238-71-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 40 percent / pyridine / 24 h / Ambient temperature

2: Et₃N / CHCl₃ / 5 h / Ambient temperature

With pyridine; triethylamine; In chloroform;

Reference yield:

L-isoleucine (73-32-5,959215-79-3,18875-42-8) → 2'-<6'-((2''S,3''S-2''-chloro-3''-methylpentanoyl)oxy)>naphthyl 4-decyloxybenzoate (143238-71-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 40 percent / aq. HCl, NaNO₂ / 4 h / 0 °C

2: SOCl₂ / benzene / Heating

3: Et₃N / CHCl₃ / 5 h / Ambient temperature

With hydrogenchloride; thionyl chloride; triethylamine; sodium nitrite; In chloroform; benzene;

Reference yield:

(2S,3S)-2-chloro-3-methylpentanoic acid (921-48-2,32644-14-7,94318-83-9,94318-84-0,95977-20-1,95977-24-5,32653-34-2) → 2'-<6'-((2''S,3''S-2''-chloro-3''-methylpentanoyl)oxy)>naphthyl 4-decyloxybenzoate (143238-71-5)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / benzene / Heating

2: Et₃N / CHCl₃ / 5 h / Ambient temperature

With thionyl chloride; triethylamine; In chloroform; benzene;

upstream raw materials:

(2S,3S)-2-chloro-3-methylpentanoyl chloride

2'-(6'-hydroxy)naphthyl 4-decyloxybenzoate

2.6-dihydroxynaphthalene

L-isoleucine