2-[2,3-dimethyl-4-(1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Base Information

Chemical Name:2-[2,3-dimethyl-4-(1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole
CAS No.:1370244-09-9
Molecular Formula:C₂₂H₂₂N₂O₄S
Molecular Weight:410.494
Hs Code.:

Synonyms:2-[2,3-dimethyl-4-(1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

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Chemical Property of 2-[2,3-dimethyl-4-(1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Chemical Property:

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Technology Process of 2-[2,3-dimethyl-4-(1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

There total 7 articles about 2-[2,3-dimethyl-4-(1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.6%

: 1370244-44-2
2-[2,3-dimethyl-4-(1-oxo-butyl)phenoxy]ethanethioamide

: 99-81-0
4-Nitrophenacyl bromide

: 1370244-09-9
2-[2,3-dimethyl-4-(1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Guidance literature:: In methanol; for 24h; Reflux;
DOI:10.1016/j.bmc.2012.02.011

Reference yield:

: 35370-84-4
2-(2,3-dimethylphenoxy)ethanethioamide

: 1370244-09-9
2-[2,3-dimethyl-4-(1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / carbon disulfide / 4.5 h / 20 - 50 °C

2: methanol / 24 h / Reflux

With aluminum (III) chloride; In methanol; carbon disulfide; 1: Friedel-Crafts acylation;
DOI:10.1016/j.bmc.2012.02.011

Reference yield:

: 35368-58-2
2-(2,3-dimethylphenoxy)acetamide

: 1370244-09-9
2-[2,3-dimethyl-4-(1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Guidance literature:: Multi-step reaction with 3 steps

1: tetraphosphorus decasulfide / tetrahydrofuran / 1.5 h / 50 °C

2: aluminum (III) chloride / carbon disulfide / 4.5 h / 20 - 50 °C

3: methanol / 24 h / Reflux

With aluminum (III) chloride; tetraphosphorus decasulfide; In tetrahydrofuran; methanol; carbon disulfide; 2: Friedel-Crafts acylation;
DOI:10.1016/j.bmc.2012.02.011