2-[2,3-dimethyl-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Base Information

Chemical Name:2-[2,3-dimethyl-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole
CAS No.:1370243-74-5
Molecular Formula:C₂₃H₂₂N₂O₄S
Molecular Weight:422.505
Hs Code.:

Synonyms:2-[2,3-dimethyl-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

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Chemical Property of 2-[2,3-dimethyl-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

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Technology Process of 2-[2,3-dimethyl-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

There total 10 articles about 2-[2,3-dimethyl-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₂₉N₃O₄S

: 1370243-74-5
2-[2,3-dimethyl-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Guidance literature:: With sodium hydrogencarbonate; In water; at 85 ℃; for 0.666667h;
DOI:10.1016/j.bmc.2012.02.011

Reference yield:

: 1370244-44-2
2-[2,3-dimethyl-4-(1-oxo-butyl)phenoxy]ethanethioamide

: 1370243-74-5
2-[2,3-dimethyl-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 24 h / Reflux

2: acetic acid / 1.5 h / 100 °C

3: sodium hydrogencarbonate / water / 0.67 h / 85 °C

With sodium hydrogencarbonate; acetic acid; In methanol; water; 2: Mannich reaction;
DOI:10.1016/j.bmc.2012.02.011

Reference yield:

: 35370-84-4
2-(2,3-dimethylphenoxy)ethanethioamide

: 1370243-74-5
2-[2,3-dimethyl-4-(2-methylene-1-oxobutyl)phenoxymethyl]-4-(4-nitrophenyl)thiazole

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum (III) chloride / carbon disulfide / 4.5 h / 20 - 50 °C

2: methanol / 24 h / Reflux

3: acetic acid / 1.5 h / 100 °C

4: sodium hydrogencarbonate / water / 0.67 h / 85 °C

With aluminum (III) chloride; sodium hydrogencarbonate; acetic acid; In methanol; carbon disulfide; water; 1: Friedel-Crafts acylation / 3: Mannich reaction;
DOI:10.1016/j.bmc.2012.02.011