2-(2,3-Dimethylphenoxy)ethanethioamide

Base Information

Chemical Name:2-(2,3-Dimethylphenoxy)ethanethioamide
CAS No.:35370-84-4
Molecular Formula:C₁₀H₁₃NOS
Molecular Weight:195.285
Hs Code.:
DSSTox Substance ID:DTXSID501284474

Synonyms:35370-84-4;Ethanethioamide, 2-(2,3-dimethylphenoxy)-;2-(2,3-dimethylphenoxy)ethanethioamide;DTXSID501284474;AKOS000197282

Suppliers and Price of 2-(2,3-Dimethylphenoxy)ethanethioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(2,3-Dimethylphenoxy)ethanethioamide

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:195.07178521
Heavy Atom Count:13
Complexity:184

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C(=CC=C1)OCC(=S)N)C

Technology Process of 2-(2,3-Dimethylphenoxy)ethanethioamide

There total 4 articles about 2-(2,3-Dimethylphenoxy)ethanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.3%

: 35368-58-2
2-(2,3-dimethylphenoxy)acetamide

: 35370-84-4
2-(2,3-dimethylphenoxy)ethanethioamide

Guidance literature:: With tetraphosphorus decasulfide; In tetrahydrofuran; at 50 ℃; for 1.5h;
DOI:10.1016/j.bmc.2012.02.011

Reference yield:

: 2935-63-9
(2,3-dimethylphenoxy)acetic acid

: 35370-84-4
2-(2,3-dimethylphenoxy)ethanethioamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 4 h / 80 °C

2: ammonia / water; toluene / 1.5 h / 0 - 5 °C

3: tetraphosphorus decasulfide / tetrahydrofuran / 1.5 h / 50 °C

With thionyl chloride; tetraphosphorus decasulfide; ammonia; In tetrahydrofuran; water; toluene;
DOI:10.1016/j.bmc.2012.02.011

Reference yield:

: 40926-74-7
2,3-Dimethyl-phenoxy-acetylchlorid

: 35370-84-4
2-(2,3-dimethylphenoxy)ethanethioamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / water; toluene / 1.5 h / 0 - 5 °C

2: tetraphosphorus decasulfide / tetrahydrofuran / 1.5 h / 50 °C

With tetraphosphorus decasulfide; ammonia; In tetrahydrofuran; water; toluene;
DOI:10.1016/j.bmc.2012.02.011