(η5-C5Me5)Ir(carbonyl)(Cl)(cyclohexyl)

Base Information

Chemical Name:(η5-C5Me5)Ir(carbonyl)(Cl)(cyclohexyl)
CAS No.:81753-17-5
Molecular Formula:C₁₇H₂₆ClIrO
Molecular Weight:474.066
Hs Code.:

Synonyms:(η5-C5Me5)Ir(carbonyl)(Cl)(cyclohexyl)

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Chemical Property of (η5-C5Me5)Ir(carbonyl)(Cl)(cyclohexyl)

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Technology Process of (η5-C5Me5)Ir(carbonyl)(Cl)(cyclohexyl)

There total 5 articles about (η5-C5Me5)Ir(carbonyl)(Cl)(cyclohexyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.1%

: 106682-39-7
(η5-C5Me5)Ir(carbonyl)(η2-p-chlorobenzonitrile)

: 110-82-7,25012-93-5
cyclohexane

: 81753-17-5
(η5-C5Me5)Ir(carbonyl)(Cl)(cyclohexyl)

: 106682-38-6
{(η5-(CH3)5cyclopentadienyl)(μ-carbonyl)iridium}2

Guidance literature:: With CCl₄; In cyclohexane; Irradiation (UV/VIS); In NMR tube, at 50°C photolyzed for 24 h under N2, evapn. addn. of CCl4 (room temp., 2 h); CCl4 removed, (1)H-NMR;

Reference yield: 48.6%

: 106712-24-7
(η5-C5Me5)(carbonyl)Ir(η2-C(p-ClC6H4)NOC(O))

: 110-82-7,25012-93-5
cyclohexane

: 81753-17-5
(η5-C5Me5)Ir(carbonyl)(Cl)(cyclohexyl)

: 106682-38-6
{(η5-(CH3)5cyclopentadienyl)(μ-carbonyl)iridium}2

Guidance literature:: With CCl₄; In cyclohexane; Irradiation (UV/VIS); Under N2, in NMR tube at 50°C, photolyzed for 13 d, metallacycle enters into soln. after about 8 d, cyclohexane is removed, cyclohexylhydride is converted to chloride deriv. by vacuum transfer of CCl4; NMR;

Reference yield: 3.0%

: 106712-24-7
(η5-C5Me5)(carbonyl)Ir(η2-C(p-ClC6H4)NOC(O))

: 110-82-7,25012-93-5
cyclohexane

: 623-03-0
4-Cyanochlorobenzene

: 81753-17-5
(η5-C5Me5)Ir(carbonyl)(Cl)(cyclohexyl)

: 106682-38-6
{(η5-(CH3)5cyclopentadienyl)(μ-carbonyl)iridium}2

Guidance literature:: With CCl₄; In cyclohexane; byproducts: CO2; Under N2, in NMR tube, for 5 weeks at 50°C in the dark, cyclohexane is removed, addn. of CCl4 converts cyclohexyl hydride to chloride deriv.; CCl4 is removed, 1H-NMR;