2-hydroxy-4-propylbenzoic acid

Base Information

Chemical Name:2-hydroxy-4-propylbenzoic acid
CAS No.:119006-58-5
Molecular Formula:C₁₀H₁₂O₃
Molecular Weight:180.203
Hs Code.:

Synonyms:2-hydroxy-4-propylbenzoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxy-4-propylbenzoic acid

Chemical Property:

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Technology Process of 2-hydroxy-4-propylbenzoic acid

There total 5 articles about 2-hydroxy-4-propylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 2-(methoxymethoxy)-4-propylbenzoic acid

: 119006-58-5
2-hydroxy-4-propylbenzoic acid

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 16h;
DOI:10.1021/acs.jmedchem.7b00785

Reference yield:

: 621-27-2
3-n-propylphenol

: 119006-58-5
2-hydroxy-4-propylbenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 0 - 100 °C

2.1: tert.-butyl lithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran; pentane; hexane / 4 h / -78 - 0 °C

2.2: 4 h / 0 °C

3.1: hydrogenchloride / 1,4-dioxane / 16 h / 20 °C

With hydrogenchloride; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; hexane; pentane;
DOI:10.1021/acs.jmedchem.7b00785

Reference yield:

: 620971-18-8
1-(methoxymethoxy)-3-propylbenzene

: 119006-58-5
2-hydroxy-4-propylbenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran; pentane; hexane / 4 h / -78 - 0 °C

1.2: 4 h / 0 °C

2.1: hydrogenchloride / 1,4-dioxane / 16 h / 20 °C

With hydrogenchloride; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium; In tetrahydrofuran; 1,4-dioxane; hexane; pentane;
DOI:10.1021/acs.jmedchem.7b00785