(S)-N-(((4-(2-(((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)carbonyl)-3-phenylsydnonimine

Base Information

Chemical Name:(S)-N-(((4-(2-(((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)carbonyl)-3-phenylsydnonimine
CAS No.:1446513-23-0
Molecular Formula:C₃₄H₂₈N₄O₇
Molecular Weight:604.619
Hs Code.:

Synonyms:(S)-N-(((4-(2-(((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)carbonyl)-3-phenylsydnonimine

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Chemical Property of (S)-N-(((4-(2-(((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)carbonyl)-3-phenylsydnonimine

Chemical Property:

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Technology Process of (S)-N-(((4-(2-(((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)carbonyl)-3-phenylsydnonimine

There total 6 articles about (S)-N-(((4-(2-(((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)carbonyl)-3-phenylsydnonimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1446512-92-0
(S)-N-((4-(2-amino-3-methoxy-3-oxopropyl)phenoxy)carbonyl)-3-phenylsydnonimine hydrochloride

: 1446513-23-0
(S)-N-(((4-(2-(((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)carbonyl)-3-phenylsydnonimine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 1h;
DOI:10.1039/c3ob41047a

Reference yield:

: 62-53-3
aniline

: 1446513-23-0
(S)-N-(((4-(2-(((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)carbonyl)-3-phenylsydnonimine

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate; sodium iodide / acetone / 12 h / 20 °C / Darkness

2.1: isopentyl nitrite / diethyl ether / 16 h / 20 °C / Darkness

2.2: 0.25 h / 20 °C

3.1: triethylamine / dichloromethane / 16 h / -20 - 20 °C

4.1: acetonitrile / 18 h / Reflux

5.1: hydrogenchloride / dichloromethane; 1,4-dioxane; water

6.1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C

With hydrogenchloride; potassium carbonate; triethylamine; sodium iodide; isopentyl nitrite; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; acetone; acetonitrile;
DOI:10.1039/c3ob41047a

Reference yield:

: 3009-97-0
N-phenylglycinonitrile

: 1446513-23-0
(S)-N-(((4-(2-(((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-methoxy-3-oxopropyl)phenoxy)carbonyl)-3-phenylsydnonimine

Guidance literature:: Multi-step reaction with 5 steps

1.1: isopentyl nitrite / diethyl ether / 16 h / 20 °C / Darkness

1.2: 0.25 h / 20 °C

2.1: triethylamine / dichloromethane / 16 h / -20 - 20 °C

3.1: acetonitrile / 18 h / Reflux

4.1: hydrogenchloride / dichloromethane; 1,4-dioxane; water

5.1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C

With hydrogenchloride; triethylamine; isopentyl nitrite; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; water; acetonitrile;
DOI:10.1039/c3ob41047a