tBuPO(NHiPr)2

Base Information

• Chemical Name: tBuPO(NHiPr)2
• CAS No.: 600116-15-2
• Molecular Formula: C₁₀H₂₅N₂OP
• Molecular Weight: 220.295

Synonyms:tBuPO(NHiPr)2

Chemical Property of tBuPO(NHiPr)2

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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Technology Process of tBuPO(NHiPr)2

There total 1 articles about tBuPO(NHiPr)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tert-butyl phosphinyl dichloride (4707-95-3) + isopropylamine (75-31-0) → isopropylamine hydrochloride (15572-56-2) + tBuPO(NHiPr)2 (600116-15-2)

Guidance literature:

In toluene; for 24h; Heating;

DOI:10.1039/b300035d

Reference yield:

diphenyltin(IV) dichloride (1135-99-5) + tBuPO(NHiPr)2 (600116-15-2) → [(C6H5)2SnCl2((CH3)3CP(O)(NHCH(CH3)2)2)2] (937262-57-2)

Guidance literature:

In toluene; soln. of Sn compd. (1 equiv.) in toluene was added to soln. of diamide (2 equiv.) in toluene at room temp.; stirred overnight; stirred at 50°C for 2 h; kept at 5°C for 12 h; elem. anal.;

DOI:10.1016/j.jorganchem.2006.12.044

Reference yield:

phenyltin trichloride (1124-19-2) + tBuPO(NHiPr)2 (600116-15-2) → [(C6H5)2SnCl2((CH3)3CP(O)(NHCH(CH3)2)2)2] (937262-57-2)

Guidance literature:

In benzene; soln. of Sn compd. (1 equiv.) in C6H6 and soln. of diamide (2 equiv.) inC6H6 were reacted;

DOI:10.1016/j.jorganchem.2006.12.044

upstream raw materials:

tert-butyl phosphinyl dichloride

isopropylamine

Downstream raw materials:

[(C₆H₅)2SnCl₂((CH₃)3CP(O)(NHCH(CH₃)2)2)2]

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