C₂₇H₃₅N₅O₃Si

Base Information

Chemical Name:C₂₇H₃₅N₅O₃Si
CAS No.:1307896-59-8
Molecular Formula:C₂₇H₃₅N₅O₃Si
Molecular Weight:505.692
Hs Code.:

C<sub>27</sub>H<sub>35</sub>N<sub>5</sub>O<sub>3</sub>Si

Synonyms:C₂₇H₃₅N₅O₃Si

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Chemical Property of C₂₇H₃₅N₅O₃Si

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Technology Process of C₂₇H₃₅N₅O₃Si

There total 8 articles about C₂₇H₃₅N₅O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 4-amino-7-(3-(tert-butyldimethylsilyloxy)propyl)-5-p-tolyl-7H-pyrrolo[2,3-d]pyrimidine-6-carbaldehyde

: 105-34-0
methyl 2-cyanoacetate

: 1307896-59-8
C₂₇H₃₅N₅O₃Si

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 1307896-57-6
methyl N-3-cyano-4-p-tolyl-1H-pyrrol-2-ylformimidate

: 1307896-59-8
C₂₇H₃₅N₅O₃Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: ammonia / methanol / 4 h / 20 °C

2.1: sodium methylate / methanol / 3 h / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

3.2: 4 h

4.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 24 h

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 3 h / Inert atmosphere

6.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 2 h / 20 °C / Inert atmosphere

7.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 1 h / 20 °C

With sodium periodate; N-Bromosuccinimide; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonia; sodium methylate; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;

Reference yield:

: 121405-36-5
5-p-tolyl-7H-pyrrolo[2,3-d]pyrimidin-4-amine

: 1307896-59-8
C₂₇H₃₅N₅O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 20 °C

1.2: 4 h

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 24 h

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 3 h / Inert atmosphere

4.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 2 h / 20 °C / Inert atmosphere

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 1 h / 20 °C

With sodium periodate; N-Bromosuccinimide; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;