ethyl rel(3S,4R)-1-benzoyl-3-(1,3-dioxolan-2-ylmethyl)piperidine-4-acetate

Base Information

Chemical Name:ethyl rel(3S,4R)-1-benzoyl-3-(1,3-dioxolan-2-ylmethyl)piperidine-4-acetate
CAS No.:83102-19-6
Molecular Formula:C₂₀H₂₇NO₅
Molecular Weight:361.438
Hs Code.:

Synonyms:ethyl rel(3S,4R)-1-benzoyl-3-(1,3-dioxolan-2-ylmethyl)piperidine-4-acetate

Suppliers and Price of ethyl rel(3S,4R)-1-benzoyl-3-(1,3-dioxolan-2-ylmethyl)piperidine-4-acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl rel(3S,4R)-1-benzoyl-3-(1,3-dioxolan-2-ylmethyl)piperidine-4-acetate

Chemical Property:

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Technology Process of ethyl rel(3S,4R)-1-benzoyl-3-(1,3-dioxolan-2-ylmethyl)piperidine-4-acetate

There total 10 articles about ethyl rel(3S,4R)-1-benzoyl-3-(1,3-dioxolan-2-ylmethyl)piperidine-4-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 98-88-4
benzoyl chloride

: 83102-16-3
ethyl rel(3S,4R)-3-(1,3-dioxolan-2-ylmethyl)piperidine-4-acetate

: 83102-19-6
ethyl rel(3S,4R)-1-benzoyl-3-(1,3-dioxolan-2-ylmethyl)piperidine-4-acetate

Guidance literature:: With potassium carbonate; In chloroform; water; for 0.0833333h; Ambient temperature;
DOI:10.1248/cpb.31.1551

Reference yield:

: 83102-07-2
benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-oxopiperidine-1-carboxylate

: 83102-19-6
ethyl rel(3S,4R)-1-benzoyl-3-(1,3-dioxolan-2-ylmethyl)piperidine-4-acetate

Guidance literature:: Multi-step reaction with 3 steps

1: benzene

2: 78 percent / H₂ / 5percent Pd/C / ethanol

3: 99 percent

With hydrogen; palladium on activated charcoal; In ethanol; benzene;
DOI:10.1248/cpb.30.1925

Reference yield:

: 83102-08-3
benzyl 3-(1,3-dioxolan-2-ylmethyl)-4-ethoxycarbonylmethylenepiperidine-1-carboxylate

: 83102-19-6
ethyl rel(3S,4R)-1-benzoyl-3-(1,3-dioxolan-2-ylmethyl)piperidine-4-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / H₂ / 5percent Pd/C / ethanol

2: 99 percent

With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1248/cpb.30.1925