N-benzyloxycarbonyl-3-aminopropyl 4,6-O-isopropylidene-β-D-glucopyranoside

Base Information

Chemical Name:N-benzyloxycarbonyl-3-aminopropyl 4,6-O-isopropylidene-β-D-glucopyranoside
CAS No.:128775-46-2
Molecular Formula:C₂₀H₂₉NO₈
Molecular Weight:411.452
Hs Code.:

Synonyms:N-benzyloxycarbonyl-3-aminopropyl 4,6-O-isopropylidene-β-D-glucopyranoside

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Chemical Property of N-benzyloxycarbonyl-3-aminopropyl 4,6-O-isopropylidene-β-D-glucopyranoside

Chemical Property:

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Technology Process of N-benzyloxycarbonyl-3-aminopropyl 4,6-O-isopropylidene-β-D-glucopyranoside

There total 4 articles about N-benzyloxycarbonyl-3-aminopropyl 4,6-O-isopropylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 120594-83-4
N-benzyloxycarbonyl-3-aminopropyl β-D-glucopyranoside

: 77-76-9
2,2-dimethoxy-propane

: 128775-46-2
N-benzyloxycarbonyl-3-aminopropyl 4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In acetone; for 4h; Ambient temperature;
DOI:10.1016/S0040-4020(01)89206-1

Reference yield:

: 14218-11-2
2,3,4,6-tetra-O-benzoylglucosyl bromide

: 128775-46-2
N-benzyloxycarbonyl-3-aminopropyl 4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / mercuric bromide, mercuric cyanide / acetonitrile / 4 h / Ambient temperature

2: 98 percent / NaOMe / methanol / 17 h / Ambient temperature

3: 79 percent / p-TsOH / acetone / 4 h / Ambient temperature

With sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; mercury dibromide; In methanol; acetone; acetonitrile;
DOI:10.1016/S0040-4020(01)89206-1

Reference yield:

: 34637-22-4
3-[(N-benzyloxycarbonyl)amino]propanol

: 128775-46-2
N-benzyloxycarbonyl-3-aminopropyl 4,6-O-isopropylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / mercuric bromide, mercuric cyanide / acetonitrile / 4 h / Ambient temperature

2: 98 percent / NaOMe / methanol / 17 h / Ambient temperature

3: 79 percent / p-TsOH / acetone / 4 h / Ambient temperature

With sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; mercury dibromide; In methanol; acetone; acetonitrile;
DOI:10.1016/S0040-4020(01)89206-1