4-Amino-thiobenzoesaeuredimethylamid

Base Information

• Chemical Name: 4-Amino-thiobenzoesaeuredimethylamid
• CAS No.: 109735-98-0
• Molecular Formula: C₉H₁₂N₂S
• Molecular Weight: 180.274

Synonyms:4-Amino-thiobenzoesaeuredimethylamid

Chemical Property of 4-Amino-thiobenzoesaeuredimethylamid

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Technology Process of 4-Amino-thiobenzoesaeuredimethylamid

There total 4 articles about 4-Amino-thiobenzoesaeuredimethylamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

4-aminobenzyl chloride (65581-19-3) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 4-Amino-thiobenzoesaeuredimethylamid (109735-98-0)

Guidance literature:

With sulfur; sodium hydroxide; at 100 ℃; for 8h; Schlenk technique;

DOI:10.1002/ejoc.202100588

Reference yield: 61.0%

4-nitrobenzeneacetic acid (104-03-0) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 4-Amino-thiobenzoesaeuredimethylamid (109735-98-0)

Guidance literature:

With potassium carbonate; sulfur; at 120 ℃; for 24h;

DOI:10.1016/j.tet.2016.02.070

Reference yield: 56.0%

4-Ethynylaniline (14235-81-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 4-Amino-thiobenzoesaeuredimethylamid (109735-98-0)

Guidance literature:

With sulfur; potassium phosphate; at 115 ℃; for 20h; Sealed tube;

DOI:10.1021/acs.orglett.8b00573

upstream raw materials:

4-nitrobenzeneacetic acid

N,N-dimethyl-formamide

4-Ethynylaniline

4-aminobenzenemethanol

Downstream raw materials:

1H-Perimidin-2-thiocarbonsaeure-(4'-dimethylaminothiocarbonylanilid)

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