(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-bis(benzyloxy)phenyl)acrylate

Base Information

Chemical Name:(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-bis(benzyloxy)phenyl)acrylate
CAS No.:1403877-27-9
Molecular Formula:C₃₇H₃₆O₈
Molecular Weight:608.688
Hs Code.:

Synonyms:(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-bis(benzyloxy)phenyl)acrylate

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Chemical Property of (E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-bis(benzyloxy)phenyl)acrylate

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Technology Process of (E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-bis(benzyloxy)phenyl)acrylate

There total 6 articles about (E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-bis(benzyloxy)phenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1322088-10-7
allyl 3-(3,4-dimethoxyphenyl)-2-hydroxypropanoate

: 54429-62-8
(E)-3-(3,4-bis(benzyloxy)phenyl)acrylic acid

: 1403877-27-9
(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-bis(benzyloxy)phenyl)acrylate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2012.09.047

Reference yield:

: 331-39-5,501-16-6
caffeic acid

: 1403877-27-9
(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-bis(benzyloxy)phenyl)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 12 h / Reflux

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / 20 °C

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; acetone;
DOI:10.1016/j.ejmech.2012.09.047

Reference yield:

: 100-39-0
benzyl bromide

: 1403877-27-9
(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-bis(benzyloxy)phenyl)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 12 h / Reflux

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / 20 °C

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; acetone;
DOI:10.1016/j.ejmech.2012.09.047