Vanillin thiosemicarbazone

Base Information

Chemical Name:Vanillin thiosemicarbazone
CAS No.:5351-92-8
Molecular Formula:C9H11 N3 O2 S
Molecular Weight:225.271
Hs Code.:
DSSTox Substance ID:DTXSID60968253
Mol file:5351-92-8.mol

Synonyms:5351-92-8;vanillin thiosemicarbazone;SCHEMBL10709406;DTXSID60968253;AKOS017263734;2-[(4-Hydroxy-3-methoxyphenyl)methylidene]hydrazine-1-carboximidothioic acid

Suppliers and Price of Vanillin thiosemicarbazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Vanillin thiosemicarbazone

Chemical Property:

Vapor Pressure:1.69E-06mmHg at 25°C
Boiling Point:396.6°Cat760mmHg
Flash Point:193.6°C
PSA：111.96000
Density:1.35g/cm³
LogP:1.65910
XLogP3:1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:225.05719778
Heavy Atom Count:15
Complexity:248

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=CC(=C1)C=NNC(=S)N)O

Technology Process of Vanillin thiosemicarbazone

There total 4 articles about Vanillin thiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.4%

: 121-33-5,8014-42-4
vanillin

: 79-19-6
thiosemicarbazide

: 5351-92-8
vanillin thiosemicarbazone

Guidance literature:: In ethanol; water; for 4h; Reflux;

Reference yield: 64.0%

: 4346-94-5
thiosemicarbazide hydrochloride

: 121-33-5,8014-42-4
vanillin

: 5351-92-8
vanillin thiosemicarbazone

Guidance literature:: With hydrogenchloride; In ethanol; water;
DOI:10.1007/s00044-012-0208-6

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 5351-92-8
vanillin thiosemicarbazone

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate; ethanol

2: acetic acid

With ethanol; potassium acetate; acetic acid;