N-[1-(4-trifluoromethoxybenzenesulfonyl)piperidin-4-yloxy]oxalamic acid

Base Information

Chemical Name:N-[1-(4-trifluoromethoxybenzenesulfonyl)piperidin-4-yloxy]oxalamic acid
CAS No.:1200798-01-1
Molecular Formula:C₁₄H₁₅F₃N₂O₇S
Molecular Weight:412.344
Hs Code.:

Synonyms:N-[1-(4-trifluoromethoxybenzenesulfonyl)piperidin-4-yloxy]oxalamic acid

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Chemical Property of N-[1-(4-trifluoromethoxybenzenesulfonyl)piperidin-4-yloxy]oxalamic acid

Chemical Property:

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Technology Process of N-[1-(4-trifluoromethoxybenzenesulfonyl)piperidin-4-yloxy]oxalamic acid

There total 7 articles about N-[1-(4-trifluoromethoxybenzenesulfonyl)piperidin-4-yloxy]oxalamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1200798-00-0
N-[1-(4-trifluoromethoxybenzenesulfonyl)piperidin-4-yloxy]oxalamic acid ethyl ester

: 1200798-01-1
N-[1-(4-trifluoromethoxybenzenesulfonyl)piperidin-4-yloxy]oxalamic acid

Guidance literature:: N-[1-(4-trifluoromethoxybenzenesulfonyl)piperidin-4-yloxy]oxalamic acid ethyl ester; With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; methanol; water;

Reference yield:

: 94108-56-2
4-(trifluoro-methoxy)benzene-1-sulfonyl chloride

: 1200798-01-1
N-[1-(4-trifluoromethoxybenzenesulfonyl)piperidin-4-yloxy]oxalamic acid

Guidance literature:: Multi-step reaction with 6 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

2: sodium tetrahydroborate; ethanol / 0 - 20 °C

3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 - 20 °C

4: hydrazine hydrate / ethanol / 2 h / 50 °C

5: triethylamine / dichloromethane / 2 h / 20 °C

6: water; sodium hydroxide / tetrahydrofuran; methanol / 1 h / 20 °C

With sodium tetrahydroborate; ethanol; water; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; dichloromethane; 3: Mitsunobu reaction;

Reference yield:

: 1092408-11-1
O-(1-(4-(trifluoromethoxy)phenylsulfonyl)piperidin-4-yl)hydroxylamine

: 1200798-01-1
N-[1-(4-trifluoromethoxybenzenesulfonyl)piperidin-4-yloxy]oxalamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 20 °C

2: water; sodium hydroxide / tetrahydrofuran; methanol / 1 h / 20 °C

With water; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;