Pyridine-2,6-dicarboxylic acid 2-[(4-methoxy-phenyl)-amide] 6-p-tolylamide

Base Information

Chemical Name:Pyridine-2,6-dicarboxylic acid 2-[(4-methoxy-phenyl)-amide] 6-p-tolylamide
CAS No.:126230-23-7
Molecular Formula:C₂₁H₁₉N₃O₃
Molecular Weight:361.4
Hs Code.:

Synonyms:Pyridine-2,6-dicarboxylic acid 2-[(4-methoxy-phenyl)-amide] 6-p-tolylamide

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Chemical Property of Pyridine-2,6-dicarboxylic acid 2-[(4-methoxy-phenyl)-amide] 6-p-tolylamide

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Technology Process of Pyridine-2,6-dicarboxylic acid 2-[(4-methoxy-phenyl)-amide] 6-p-tolylamide

There total 3 articles about Pyridine-2,6-dicarboxylic acid 2-[(4-methoxy-phenyl)-amide] 6-p-tolylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 201230-82-2
carbon monoxide

: 104-94-9
4-methoxy-aniline

: 126230-15-7
N-(4-methylphenyl)-6-bromopyridine-2-carboxamide

: 126230-23-7
Pyridine-2,6-dicarboxylic acid 2-[(4-methoxy-phenyl)-amide] 6-p-tolylamide

Guidance literature:: With triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 100 ℃; for 5h; under 2574.3 Torr;
DOI:10.1055/s-1989-27372

Reference yield:

: 626-05-1
2,6-Dibromopyridine

: 126230-23-7
Pyridine-2,6-dicarboxylic acid 2-[(4-methoxy-phenyl)-amide] 6-p-tolylamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / Pd(PPh₃)4 / toluene / 5 h / 100 °C / 2206.5 Torr

2: 59 percent / Et₃N / Pd(PPh₃)4 / toluene / 5 h / 100 °C / 2574.3 Torr

With triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;
DOI:10.1055/s-1989-27372

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 126230-23-7
Pyridine-2,6-dicarboxylic acid 2-[(4-methoxy-phenyl)-amide] 6-p-tolylamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / Pd(PPh₃)4 / toluene / 5 h / 100 °C / 2206.5 Torr

2: 59 percent / Et₃N / Pd(PPh₃)4 / toluene / 5 h / 100 °C / 2574.3 Torr

With triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;
DOI:10.1055/s-1989-27372