1,3-bis((S)-2,2-dimethyl-1-(naphthalen-1-yl)propyl)-4,5-dihydro-1H-imidazol-3-ium iodide

Base Information

Chemical Name:1,3-bis((S)-2,2-dimethyl-1-(naphthalen-1-yl)propyl)-4,5-dihydro-1H-imidazol-3-ium iodide
CAS No.:1333385-97-9
Molecular Formula:C₃₃H₃₉N₂*I
Molecular Weight:590.591
Hs Code.:

Synonyms:1,3-bis((S)-2,2-dimethyl-1-(naphthalen-1-yl)propyl)-4,5-dihydro-1H-imidazol-3-ium iodide

Suppliers and Price of 1,3-bis((S)-2,2-dimethyl-1-(naphthalen-1-yl)propyl)-4,5-dihydro-1H-imidazol-3-ium iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
1,3-Bis[(1S)-2,2-dimethyl-1-(1-naphthyl)propyl]imidazolinium iodide ≥96% (HPLC)
100mg
$ 246.00

Alichem
1,3-Bis((S)-2,2-dimethyl-1-(naphthalen-1-yl)propyl)-4,5-dihydro-1H-imidazol-3-iumiodide
100mg
$ 400.00

Total 2 raw suppliers

Chemical Property of 1,3-bis((S)-2,2-dimethyl-1-(naphthalen-1-yl)propyl)-4,5-dihydro-1H-imidazol-3-ium iodide

Chemical Property:

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,3-Bis[(1S)-2,2-dimethyl-1-(1-naphthyl)propyl]imidazolinium iodide ≥96% (HPLC) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses Carbene ligand precursor

Technology Process of 1,3-bis((S)-2,2-dimethyl-1-(naphthalen-1-yl)propyl)-4,5-dihydro-1H-imidazol-3-ium iodide

There total 5 articles about 1,3-bis((S)-2,2-dimethyl-1-(naphthalen-1-yl)propyl)-4,5-dihydro-1H-imidazol-3-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄H₆O₅*C₁₅H₁₉N

: 1333385-97-9
1,3-bis((S)-2,2-dimethyl-1-(naphthalen-1-yl)propyl)-4,5-dihydro-1H-imidazol-3-ium iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / diethyl ether; water

2.1: formic acid; sodium sulfate / dichloromethane / 5 h / 25 °C

2.2: 0 - 25 °C / Inert atmosphere

2.3: 12 h / 125 °C

3.1: sodium iodide / acetone

With formic acid; sodium sulfate; sodium iodide; sodium hydroxide; In diethyl ether; dichloromethane; water; acetone;
DOI:10.1002/chem.201301572

Reference yield:

: 324034-56-2
α-(1,1-Dimethylethyl)-1-naphthalinmethanamin

: 1333385-97-9
1,3-bis((S)-2,2-dimethyl-1-(naphthalen-1-yl)propyl)-4,5-dihydro-1H-imidazol-3-ium iodide

Guidance literature:: Multi-step reaction with 4 steps

1.1: isopropyl alcohol; ethyl acetate / 1 h / 100 °C / Resolution of racemate

2.1: sodium hydroxide / diethyl ether; water

3.1: formic acid; sodium sulfate / dichloromethane / 5 h / 25 °C

3.2: 0 - 25 °C / Inert atmosphere

3.3: 12 h / 125 °C

4.1: sodium iodide / acetone

With formic acid; sodium sulfate; sodium iodide; sodium hydroxide; In diethyl ether; dichloromethane; water; ethyl acetate; isopropyl alcohol; acetone;
DOI:10.1002/chem.201301572

Reference yield:

: 86-53-3
1-Cyanonaphthalene

: 1333385-97-9
1,3-bis((S)-2,2-dimethyl-1-(naphthalen-1-yl)propyl)-4,5-dihydro-1H-imidazol-3-ium iodide

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(I) bromide / diethyl ether / 24 h / Inert atmosphere; Reflux

1.2: 16 h / -78 - 25 °C / Inert atmosphere

2.1: isopropyl alcohol; ethyl acetate / 1 h / 100 °C / Resolution of racemate

3.1: sodium hydroxide / diethyl ether; water

4.1: formic acid; sodium sulfate / dichloromethane / 5 h / 25 °C

4.2: 0 - 25 °C / Inert atmosphere

4.3: 12 h / 125 °C

5.1: sodium iodide / acetone

With formic acid; sodium sulfate; sodium iodide; copper(I) bromide; sodium hydroxide; In diethyl ether; dichloromethane; water; ethyl acetate; isopropyl alcohol; acetone;
DOI:10.1002/chem.201301572