4-(4-((5-chloro-2-oxoindolin-3-yliden)methyl)-2-methoxyphenoxy)butanitrile

Base Information

Chemical Name:4-(4-((5-chloro-2-oxoindolin-3-yliden)methyl)-2-methoxyphenoxy)butanitrile
CAS No.:1415609-39-0
Molecular Formula:C₂₀H₁₇ClN₂O₃
Molecular Weight:368.82
Hs Code.:

Synonyms:4-(4-((5-chloro-2-oxoindolin-3-yliden)methyl)-2-methoxyphenoxy)butanitrile

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Chemical Property of 4-(4-((5-chloro-2-oxoindolin-3-yliden)methyl)-2-methoxyphenoxy)butanitrile

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Technology Process of 4-(4-((5-chloro-2-oxoindolin-3-yliden)methyl)-2-methoxyphenoxy)butanitrile

There total 2 articles about 4-(4-((5-chloro-2-oxoindolin-3-yliden)methyl)-2-methoxyphenoxy)butanitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 17630-75-0
5-chloro-indolin-2-one

: 928711-58-4
4-(4-formyl-2-methoxyphenoxy)butanitrile

: 1415609-39-0
4-(4-((5-chloro-2-oxoindolin-3-yliden)methyl)-2-methoxyphenoxy)butanitrile

Guidance literature:: With piperidine; In methanol; at 100 ℃; for 0.5h; Microwave irradiation;
DOI:10.1016/j.bmcl.2012.10.016

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1415609-39-0
4-(4-((5-chloro-2-oxoindolin-3-yliden)methyl)-2-methoxyphenoxy)butanitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / 70 °C

2: piperidine / methanol / 0.5 h / 100 °C / Microwave irradiation

With piperidine; potassium carbonate; In methanol; 2: |Knoevenagel Condensation;
DOI:10.1016/j.bmcl.2012.10.016