di(tert-butyl)difluoro[4-(3-oxo-2,3-diphenylpropyl)phenyl]methylphosphonate

Base Information

Chemical Name:di(tert-butyl)difluoro[4-(3-oxo-2,3-diphenylpropyl)phenyl]methylphosphonate
CAS No.:345953-50-6
Molecular Formula:C₃₀H₃₅F₂O₄P
Molecular Weight:528.576
Hs Code.:

Synonyms:di(tert-butyl)difluoro[4-(3-oxo-2,3-diphenylpropyl)phenyl]methylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(tert-butyl)difluoro[4-(3-oxo-2,3-diphenylpropyl)phenyl]methylphosphonate

Chemical Property:

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Technology Process of di(tert-butyl)difluoro[4-(3-oxo-2,3-diphenylpropyl)phenyl]methylphosphonate

There total 1 articles about di(tert-butyl)difluoro[4-(3-oxo-2,3-diphenylpropyl)phenyl]methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 451-40-1
phenyl benzyl ketone

: 261176-00-5
(4-bromomethylphenyl) difluoromethylphosphonic acid di-tert-butyl ester

: 345953-50-6
di(tert-butyl)difluoro[4-(3-oxo-2,3-diphenylpropyl)phenyl]methylphosphonate

Guidance literature:: phenyl benzyl ketone; With sodium hydride; In N,N-dimethyl-formamide;

(4-bromomethylphenyl) difluoromethylphosphonic acid di-tert-butyl ester; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2003.11.048

Reference yield:

: 345953-50-6
di(tert-butyl)difluoro[4-(3-oxo-2,3-diphenylpropyl)phenyl]methylphosphonate

: 261175-36-4
[4-(2-{4-[difluoro(phosphono)methyl]benzyl}-3-oxo-2,3-diphenylpropyl)phenyl](difluoro)methylphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butoxide / tetrahydrofuran

1.2: tetrahydrofuran

2.1: aq. AcOH

With potassium tert-butylate; acetic acid; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2003.11.048

Reference yield:

: 261176-00-5
(4-bromomethylphenyl) difluoromethylphosphonic acid di-tert-butyl ester

: 345953-50-6
di(tert-butyl)difluoro[4-(3-oxo-2,3-diphenylpropyl)phenyl]methylphosphonate

: 261176-45-8
Di(tert-butyl)[4-(2-{4-[[di(tert-butoxy)phosphoryl](difluoro)methyl]benzyl}-3-oxo-2,3-diphenylpropyl)phenyl](difluoro)methylphosphonate

Guidance literature:: di(tert-butyl)difluoro[4-(3-oxo-2,3-diphenylpropyl)phenyl]methylphosphonate; With potassium tert-butylate; In tetrahydrofuran;

(4-bromomethylphenyl) difluoromethylphosphonic acid di-tert-butyl ester; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2003.11.048