10-(4-chlorobenzylidene)-7-phenyl-5,7-dihydro-6H-benzo[h][1,3]thiazolo[2,3-b]quinazolin-9(10H)-one

Base Information

Chemical Name:10-(4-chlorobenzylidene)-7-phenyl-5,7-dihydro-6H-benzo[h][1,3]thiazolo[2,3-b]quinazolin-9(10H)-one
CAS No.:1141934-87-3
Molecular Formula:C₂₇H₁₉ClN₂OS
Molecular Weight:454.98
Hs Code.:
Mol file:1141934-87-3.mol

Synonyms:(E)-10-(4-chlorobenzylidene)-7-phenyl-7,10-dihydro-5H-benzo[h]thiazolo[2,3-b]quinazolin-9(6H)-one

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Chemical Property of 10-(4-chlorobenzylidene)-7-phenyl-5,7-dihydro-6H-benzo[h][1,3]thiazolo[2,3-b]quinazolin-9(10H)-one

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Technology Process of 10-(4-chlorobenzylidene)-7-phenyl-5,7-dihydro-6H-benzo[h][1,3]thiazolo[2,3-b]quinazolin-9(10H)-one

There total 6 articles about 10-(4-chlorobenzylidene)-7-phenyl-5,7-dihydro-6H-benzo[h][1,3]thiazolo[2,3-b]quinazolin-9(10H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 104-88-1
4-chlorobenzaldehyde

: 153258-17-4
5H-5-phenyl-6,7-dihydrothiazolo<2,3-b>benzoquinazolin-3(2H)-one

: 1141934-87-3
(E)-10-(4-chlorobenzylidene)-7-phenyl-7,10-dihydro-5H-benzo[h]thiazolo[2,3-b]quinazolin-9(6H)-one

Guidance literature:: With sodium acetate; acetic acid; for 4h; Reflux;
DOI:10.1016/j.molstruc.2013.06.038

Reference yield: 66.0%

: 104-88-1
4-chlorobenzaldehyde

: 85660-18-0
3,4,6,7-tetrahydro-4-phenylbenzoquinazolin-2(1H)-thione

: 79-11-8
chloroacetic acid

: 1141934-87-3
(E)-10-(4-chlorobenzylidene)-7-phenyl-7,10-dihydro-5H-benzo[h]thiazolo[2,3-b]quinazolin-9(6H)-one

Guidance literature:: With sodium acetate; acetic anhydride; acetic acid; Reflux;
DOI:10.1016/j.molstruc.2013.06.038

Reference yield:

: 17216-08-9
2-acetyl-1-tetralone

: 1141934-87-3
(E)-10-(4-chlorobenzylidene)-7-phenyl-7,10-dihydro-5H-benzo[h]thiazolo[2,3-b]quinazolin-9(6H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide; acetic acid / ethanol / 4 h / Reflux

2: sodium acetate; acetic acid; acetic anhydride / Reflux

With sodium acetate; acetic anhydride; acetic acid; potassium hydroxide; In ethanol;
DOI:10.1016/j.molstruc.2013.06.038