C₁₅H₂₄O₅SSi

Base Information Edit

Chemical Name:C₁₅H₂₄O₅SSi
CAS No.:1384626-91-8
Molecular Formula:C₁₅H₂₄O₅SSi
Molecular Weight:344.504
Hs Code.:
Mol file:1384626-91-8.mol

C<sub>15</sub>H<sub>24</sub>O<sub>5</sub>SSi

Synonyms:C₁₅H₂₄O₅SSi

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Chemical Property of C₁₅H₂₄O₅SSi Edit

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Technology Process of C₁₅H₂₄O₅SSi

There total 4 articles about C₁₅H₂₄O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 1384626-91-8
C₁₅H₂₄O₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2: AD-mix α; methanesulfonamide; water / tert-butyl alcohol / 9.5 h / 0 °C

3: thionyl chloride; triethylamine / dichloromethane / 0.17 h / 0 °C

4: sodium periodate; ruthenium(III) chloride trihydrate / tetrachloromethane; water; acetonitrile / 1 h / 0 °C

With 1H-imidazole; sodium periodate; thionyl chloride; methanesulfonamide; ruthenium(III) chloride trihydrate; AD-mix α; water; triethylamine; In tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetasy.2012.04.018

Reference yield:

: (1S,2S)-3-(tert-butyldimethylsilyloxy)-1-phenylpropane-1,2-diol

: 1384626-91-8
C₁₅H₂₄O₅SSi

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; triethylamine / dichloromethane / 0.17 h / 0 °C

2: sodium periodate; ruthenium(III) chloride trihydrate / tetrachloromethane; water; acetonitrile / 1 h / 0 °C

With sodium periodate; thionyl chloride; ruthenium(III) chloride trihydrate; triethylamine; In tetrachloromethane; dichloromethane; water; acetonitrile;
DOI:10.1016/j.tetasy.2012.04.018

Reference yield:

: 100009-29-8
(E)-1-tert-butyldimethylsilyloxy-3-phenyl-2-propene

: 1384626-91-8
C₁₅H₂₄O₅SSi

Guidance literature:: Multi-step reaction with 3 steps

1: AD-mix α; methanesulfonamide; water / tert-butyl alcohol / 9.5 h / 0 °C

2: thionyl chloride; triethylamine / dichloromethane / 0.17 h / 0 °C

3: sodium periodate; ruthenium(III) chloride trihydrate / tetrachloromethane; water; acetonitrile / 1 h / 0 °C

With sodium periodate; thionyl chloride; methanesulfonamide; ruthenium(III) chloride trihydrate; AD-mix α; water; triethylamine; In tetrachloromethane; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetasy.2012.04.018