Diisopropyl-((E)-3-phenyl-allyloxy)-((Z)-3-phenyl-allyloxy)-silane

Base Information

• Chemical Name: Diisopropyl-((E)-3-phenyl-allyloxy)-((Z)-3-phenyl-allyloxy)-silane
• CAS No.: 158956-31-1
• Molecular Formula: C₂₄H₃₂O₂Si
• Molecular Weight: 380.602
• Mol file: 158956-31-1.mol

Synonyms:Diisopropyl-((E)-3-phenyl-allyloxy)-((Z)-3-phenyl-allyloxy)-silane

Chemical Property of Diisopropyl-((E)-3-phenyl-allyloxy)-((Z)-3-phenyl-allyloxy)-silane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Diisopropyl-((E)-3-phenyl-allyloxy)-((Z)-3-phenyl-allyloxy)-silane

There total 3 articles about Diisopropyl-((E)-3-phenyl-allyloxy)-((Z)-3-phenyl-allyloxy)-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2E)-3-phenyl-2-propen-1-ol (4407-36-7) → Diisopropyl-((E)-3-phenyl-allyloxy)-((Z)-3-phenyl-allyloxy)-silane (158956-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / Et₃N / CH₂Cl₂ / 10 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 10 h

With triethylamine; In dichloromethane;

DOI:10.1021/jo00100a063

Reference yield:

Diisopropylsilyl dichloride (7751-38-4) → Diisopropyl-((E)-3-phenyl-allyloxy)-((Z)-3-phenyl-allyloxy)-silane (158956-31-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / Et₃N / CH₂Cl₂ / 10 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 10 h

With triethylamine; In dichloromethane;

DOI:10.1021/jo00100a063

Reference yield:

(Z)-cinnamyl alcohol (4510-34-3) + diisopropyl(cinnamyloxy)silyl chloride (158956-25-3) → Diisopropyl-((E)-3-phenyl-allyloxy)-((Z)-3-phenyl-allyloxy)-silane (158956-31-1)

Guidance literature:

With triethylamine; In dichloromethane; for 10h; Yield given;

DOI:10.1021/jo00100a063

upstream raw materials:

(Z)-cinnamyl alcohol

diisopropyl(cinnamyloxy)silyl chloride

Diisopropylsilyl dichloride

(2E)-3-phenyl-2-propen-1-ol

Downstream raw materials:

1,2-Bis(hydroxymethyl)-3,4-diphenylcyclobutane