3-(Acetylamino)-1,2,4-benzotriazine 1,4-dioxide

Base Information

Chemical Name:3-(Acetylamino)-1,2,4-benzotriazine 1,4-dioxide
CAS No.:27315-02-2
Molecular Formula:C9H8 N4 O3
Molecular Weight:220.188
Hs Code.:
Mol file:27315-02-2.mol

Synonyms:Acetamide,N-1,2,4-benzotriazin-3-yl-, 1,4-dioxide (8CI); Acetamide, N-1,2,4-benzotriazin-3-yl-,N,N'-dioxide; 1,2,4-Benzotriazine, acetamide deriv.; NSC 613693; SR 4452

Suppliers and Price of 3-(Acetylamino)-1,2,4-benzotriazine 1,4-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-(Acetylamino)-1,2,4-benzotriazine 1,4-dioxide

Chemical Property:

Melting Point:200 °C
PKA:9.92±0.43(Predicted)
PSA：92.94000
Density:1.545g/cm³
LogP:0.14930

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(Acetylamino)-1,2,4-benzotriazine 1,4-dioxide

There total 3 articles about 3-(Acetylamino)-1,2,4-benzotriazine 1,4-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.8%

: 27314-97-2
3-amino-1,2,4-benzotriazine-1,4-dioxide

: 108-24-7
acetic anhydride

: 27315-02-2
3-acetylamino-1,2,4-benzotriazine-1,4-dioxide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 3h; under 760.051 Torr; Sonication; Cooling with ice;

Reference yield:

: 480-96-6,68100-26-5
benzofurazan oxide

: 27315-02-2
3-acetylamino-1,2,4-benzotriazine-1,4-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / water; methanol / 4 h / 60 °C

1.2: pH 5 - 8

2.1: triethylamine / tetrahydrofuran / 3 h / 20 °C / 760.05 Torr / Sonication; Cooling with ice

With triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; water;