4,7-diphenoxy-1,10-phenanthroline

Base Information

Chemical Name:4,7-diphenoxy-1,10-phenanthroline
CAS No.:95943-00-3
Molecular Formula:C₂₄H₁₆N₂O₂
Molecular Weight:364.403
Hs Code.:

Synonyms:4,7-diphenoxy-1,10-phenanthroline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,7-diphenoxy-1,10-phenanthroline

Chemical Property:

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Technology Process of 4,7-diphenoxy-1,10-phenanthroline

There total 2 articles about 4,7-diphenoxy-1,10-phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 5394-23-0
4,7-dichloro-1,10-phenanthroline

: 108-95-2,27073-41-2
phenol

: 95943-00-3
4,7-diphenoxy-1,10-phenanthroline

Guidance literature:: With potassium hydroxide; at 120 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jacs.0c00727

Reference yield:

: 95943-00-3
4,7-diphenoxy-1,10-phenanthroline

Guidance literature:: 4,7-Dichlor-1,10-phenanthrolin, Erhitzen mit Phenol u. KOH;

Reference yield: 95.0%

: ferrous(II) sulfate heptahydrate

: ammonium hexafluorophosphate

: 95943-00-3
4,7-diphenoxy-1,10-phenanthroline

: tris(4,7-diphenoxy-1,10-phenanthroline)iron(II) hexafluorophosphate

Guidance literature:: In water; acetonitrile; the phenanthroline was added to a soln. of the Fe(2+)-salt in water; the suspension was sonicated with ultrasound for 30 min at 60 ° CN addn. of CH3CN gave a clear soln.; precipitation of the product upon addn. of NH4PF6;; filtration; washing with water; drying at 120 ° C in vacuo;;