cis ethyl 4-(piperidin-4-yloxy)cyclohexanecarboxylate

Base Information

Chemical Name:cis ethyl 4-(piperidin-4-yloxy)cyclohexanecarboxylate
CAS No.:1415573-47-5
Molecular Formula:C₁₄H₂₅NO₃
Molecular Weight:255.357
Hs Code.:

Synonyms:cis ethyl 4-(piperidin-4-yloxy)cyclohexanecarboxylate

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Chemical Property of cis ethyl 4-(piperidin-4-yloxy)cyclohexanecarboxylate

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Technology Process of cis ethyl 4-(piperidin-4-yloxy)cyclohexanecarboxylate

There total 8 articles about cis ethyl 4-(piperidin-4-yloxy)cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1614234-61-5
cis benzyl-4-(4-(ethoxycarbonyl)cyclohexyloxy)piperidine-1-carboxylate

: 1415573-47-5
cis ethyl 4-(piperidin-4-yloxy)cyclohexanecarboxylate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; ethyl acetate; under 1034.32 Torr; diastereoselective reaction;
DOI:10.1016/j.tet.2014.04.064

Reference yield:

: 3618-04-0,75877-66-6,17159-80-7
4-hydroxycyclohexyl carboxylic acid ethyl ester

: 1415573-47-5
cis ethyl 4-(piperidin-4-yloxy)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 48 h / 55 °C

2: ChiralPak AD-H / Resolution of racemate

3: hydrogen; acetic acid / platinum(IV) oxide

With di-isopropyl azodicarboxylate; hydrogen; acetic acid; triphenylphosphine; platinum(IV) oxide; In tetrahydrofuran;

Reference yield:

: 626-64-2,157061-69-3
pyridin-4-ol

: 1415573-47-5
cis ethyl 4-(piperidin-4-yloxy)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 48 h / 55 °C

2: ChiralPak AD-H / Resolution of racemate

3: hydrogen; acetic acid / platinum(IV) oxide

With di-isopropyl azodicarboxylate; hydrogen; acetic acid; triphenylphosphine; platinum(IV) oxide; In tetrahydrofuran;