O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-1,5,6-tri-O-benzyl-L-myo-inositol

Base Information

Chemical Name:O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-1,5,6-tri-O-benzyl-L-myo-inositol
CAS No.:133163-53-8
Molecular Formula:C₅₄H₅₇N₃O₁₀
Molecular Weight:908.061
Hs Code.:

Synonyms:O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-1,5,6-tri-O-benzyl-L-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-1,5,6-tri-O-benzyl-L-myo-inositol

Chemical Property:

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Technology Process of O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-1,5,6-tri-O-benzyl-L-myo-inositol

There total 27 articles about O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-1,5,6-tri-O-benzyl-L-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->6)-3,4,5-tri-O-benzyl-1,2-O-(L-1,7,7-trimethyl<2.2.1>bicyclohept-6-ylidene)-D-myo-inositol

: 133163-53-8
O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-1,5,6-tri-O-benzyl-L-myo-inositol

Guidance literature:: With water; trifluoroacetic acid; In chloroform; for 6h;
DOI:10.1002/(SICI)1521-3765(19990104)5:1<320::AID-CHEM320>3.0.CO;2-K

Reference yield: 39.0%

: C₆₀H₆₅N₃O₁₀

: 133163-53-8
O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-1,5,6-tri-O-benzyl-L-myo-inositol

: (1R,2S,3R,4R,5S,6R)-3-((2R,3R,4R,5S,6R)-3-Azido-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-4,5,6-tris-benzyloxy-cyclohexane-1,2-diol

Guidance literature:: With hydrogenchloride; In methanol; dichloromethane;

Reference yield:

: 55682-48-9
1,6-anhydro-2-azido-3,4-di-O-benzyl-2-deoxy-D-glucopyranose

: 133163-53-8
O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-1,5,6-tri-O-benzyl-L-myo-inositol

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / 10percent CF₃COOH

2: 1. H₂NNH₂*HOAc 2. K₂CO₃ / 1. DMF 2. CH₂Cl₂

3: 84 percent / trimethylsilyl triflate, MS (4 Angstroem) / CH₂Cl₂ / -20 °C

4: 1. NaOMe 2. NaH, Bu₄NI / 1. MeOH/CH₂Cl₂ 2. DMF

5: 43 percent / HCl / methanol; CH₂Cl₂

With hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; MS (4 Angstroem); sodium methylate; hydrazinium monoacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; trifluoroacetic acid; In methanol; dichloromethane;