(3R,4R)-(+)-3,4-heptanediol

Base Information

• Chemical Name: (3R,4R)-(+)-3,4-heptanediol
• CAS No.: 130272-06-9
• Molecular Formula: C₇H₁₆O₂
• Molecular Weight: 132.203
• Mol file: 130272-06-9.mol

Synonyms:(3R,4R)-(+)-3,4-heptanediol

Chemical Property of (3R,4R)-(+)-3,4-heptanediol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (3R,4R)-(+)-3,4-heptanediol

There total 8 articles about (3R,4R)-(+)-3,4-heptanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-3-heptene (7642-10-6) → (+/-)-erythro-heptane-3,4-diol (62593-33-3,121862-06-4,121862-07-5,130272-06-9)

Guidance literature:

With osmium(VIII) oxide; N-methyl-2-indolinone; In acetone; at 0 ℃; for 12h; Yield given;

DOI:10.1039/a704812b

Reference yield:

n-heptane (142-82-5) → (+/-)-erythro-heptane-3,4-diol (62593-33-3,121862-06-4,121862-07-5,130272-06-9) + 1,2-heptanediol (3710-31-4) + (2RS,3SR)-heptane-2,3-diol + (2RS,3RS)-heptane-2,3-diol + (3R,4R)-Heptane-3,4-diol

Guidance literature:

n-heptane; With peracetic acid; sodium azide; 4-tolyl iodide; iodine; acetic acid; at 20 ℃; for 24h;

With lithium hydroxide; In methanol; at 20 ℃;

DOI:10.1039/C6SC03055F

Reference yield:

→ (+/-)-erythro-heptane-3,4-diol (62593-33-3,121862-06-4,121862-07-5,130272-06-9)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

upstream raw materials:

(Z)-3-heptene

n-heptane

cis-2-ethyl-3-propyloxirane

(3R)-(+)-3-(isopropoxydimethylsilyl)-4-heptanone