Dimethyl 2,2-dibenzylmalonate

Base Information

Chemical Name:Dimethyl 2,2-dibenzylmalonate
CAS No.:72013-65-1
Molecular Formula:C₁₉H₂₀O₄
Molecular Weight:312.365
Hs Code.:

Synonyms:Dimethyl 2,2-dibenzylmalonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl 2,2-dibenzylmalonate

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Dimethyl 2,2-dibenzylmalonate

There total 8 articles about Dimethyl 2,2-dibenzylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 100-39-0
benzyl bromide

: 108-59-8
malonic acid dimethyl ester

: 72013-65-1
Dimethyl 2,2-dibenzylmalonate

Guidance literature:: With C₁₂H₂₀F₃N₂S⁽¹⁺⁾*BF₄^(1-); potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 10h;
DOI:10.1039/c6ra06870g

Reference yield: 83.0%

: 108-59-8
malonic acid dimethyl ester

: 100-51-6,185532-71-2
benzyl alcohol

: 72013-65-1
Dimethyl 2,2-dibenzylmalonate

Guidance literature:: With 1,3-bis-(diphenylphosphino)propane; palladium diacetate; caesium carbonate; carbonic acid dimethyl ester; In neat liquid; at 120 ℃; for 36h; Concentration; Solvent; Time; Reagent/catalyst; Inert atmosphere;
DOI:10.1039/c6gc00163g

Reference yield: 59.0%

: 140-11-4
Benzyl acetate

: 108-59-8
malonic acid dimethyl ester

: 49769-78-0
2-benzyl-malonic acid dimethyl ester

: 72013-65-1
Dimethyl 2,2-dibenzylmalonate

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; potassium carbonate; [Pd(η3-C3H5)(cod)]BF4; In tert-Amyl alcohol; at 80 ℃; for 3h; Further Variations:; Solvents; Reagents; Product distribution;
DOI:10.1016/j.tetlet.2007.06.157