N-<1-(3,4-dimethoxy-6-iodophenyl)but-3-en-1-yl>-5,5-dimethoxypentanamide

Base Information

Chemical Name:N-<1-(3,4-dimethoxy-6-iodophenyl)but-3-en-1-yl>-5,5-dimethoxypentanamide
CAS No.:80696-85-1
Molecular Formula:C₁₉H₂₈INO₅
Molecular Weight:477.34
Hs Code.:

Synonyms:N-<1-(3,4-dimethoxy-6-iodophenyl)but-3-en-1-yl>-5,5-dimethoxypentanamide

Suppliers and Price of N-<1-(3,4-dimethoxy-6-iodophenyl)but-3-en-1-yl>-5,5-dimethoxypentanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<1-(3,4-dimethoxy-6-iodophenyl)but-3-en-1-yl>-5,5-dimethoxypentanamide

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Technology Process of N-<1-(3,4-dimethoxy-6-iodophenyl)but-3-en-1-yl>-5,5-dimethoxypentanamide

There total 2 articles about N-<1-(3,4-dimethoxy-6-iodophenyl)but-3-en-1-yl>-5,5-dimethoxypentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61203-53-0
2-iodo-4,5-dimethoxybenzaldehyde

: 80696-85-1
N-<1-(3,4-dimethoxy-6-iodophenyl)but-3-en-1-yl>-5,5-dimethoxypentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) hexamethyldisilazane, n-butyllithium / 1.) THF, hexane, RT, 1 h, 2.) ether, RT, 20 min

2: 1.) trimethylaluminum / 1.) dichloromethane + heptane, RT, 30 min, 2.) reflux, 20 h

With n-butyllithium; trimethylaluminum; 1,1,1,3,3,3-hexamethyl-disilazane;
DOI:10.1021/jo00347a036

Reference yield:

: 23068-91-9
methyl 5,5-dimethoxyvalerate

: 83948-32-7
4-amino-4-(3,4-dimethoxy-6-iodophenyl)-1-butene

: 80696-85-1
N-<1-(3,4-dimethoxy-6-iodophenyl)but-3-en-1-yl>-5,5-dimethoxypentanamide

Guidance literature:: With trimethylaluminum; Yield given. Multistep reaction; 1.) dichloromethane + heptane, RT, 30 min, 2.) reflux, 20 h;
DOI:10.1021/jo00347a036