{(R)-2-hydroxy-1-[4-((S)-2-methyl-butoxy)phenyl]ethyl}amine hydrochloride

Base Information

Chemical Name:{(R)-2-hydroxy-1-[4-((S)-2-methyl-butoxy)phenyl]ethyl}amine hydrochloride
CAS No.:1286280-52-1
Molecular Formula:C₁₃H₂₁NO₂*ClH
Molecular Weight:259.776
Hs Code.:

Synonyms:{(R)-2-hydroxy-1-[4-((S)-2-methyl-butoxy)phenyl]ethyl}amine hydrochloride

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Chemical Property of {(R)-2-hydroxy-1-[4-((S)-2-methyl-butoxy)phenyl]ethyl}amine hydrochloride

Chemical Property:

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Technology Process of {(R)-2-hydroxy-1-[4-((S)-2-methyl-butoxy)phenyl]ethyl}amine hydrochloride

There total 7 articles about {(R)-2-hydroxy-1-[4-((S)-2-methyl-butoxy)phenyl]ethyl}amine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1286280-51-0
{(R)-2-hydroxy-1-[4-((S)-2-methyl-butoxy)phenyl]ethyl}carbamic acid t-butyl ester

: 1286280-52-1
{(R)-2-hydroxy-1-[4-((S)-2-methyl-butoxy)phenyl]ethyl}amine hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 2h; Cooling with ice;

Reference yield:

: 36438-64-9
p-benzyloxystyrene

: 1286280-52-1
{(R)-2-hydroxy-1-[4-((S)-2-methyl-butoxy)phenyl]ethyl}amine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide; tert-butylhypochlorite / water; propan-1-ol / 0.08 h / 20 °C

1.2: 0.1 h / Cooling with ice

1.3: 1.5 h / 0 °C

2.1: hydrogen / palladium on carbon / dichloromethane; ethanol / 20 °C / 760.05 Torr

3.1: caesium carbonate / N,N-dimethyl-formamide / 70 °C

4.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 2 h / 20 °C / Cooling with ice

With hydrogenchloride; tert-butylhypochlorite; hydrogen; caesium carbonate; sodium hydroxide; palladium on carbon; In 1,4-dioxane; propan-1-ol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 4397-53-9
p-benzyloxybenzaldehyde

: 1286280-52-1
{(R)-2-hydroxy-1-[4-((S)-2-methyl-butoxy)phenyl]ethyl}amine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: 3 h / 0 - 20 °C

2.1: sodium hydroxide; tert-butylhypochlorite / water; propan-1-ol / 0.08 h / 20 °C

2.2: 0.1 h / Cooling with ice

2.3: 1.5 h / 0 °C

3.1: hydrogen / palladium on carbon / dichloromethane; ethanol / 20 °C / 760.05 Torr

4.1: caesium carbonate / N,N-dimethyl-formamide / 70 °C

5.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 2 h / 20 °C / Cooling with ice

With hydrogenchloride; n-butyllithium; tert-butylhypochlorite; hydrogen; caesium carbonate; sodium hydroxide; palladium on carbon; In tetrahydrofuran; 1,4-dioxane; propan-1-ol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;