Technology Process of C30H30O8
There total 5 articles about C30H30O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-methoxyphenyl 1-α-D-rhamnopyranoside;
With
di(n-butyl)tin oxide;
In
tetrahydrofuran; toluene;
for 2h;
Heating;
allyl bromide;
tetrabutylammomium bromide;
In
toluene;
at 65 ℃;
for 12h;
benzoyl chloride;
With
pyridine;
at 0 - 20 ℃;
for 12h;
DOI:10.1016/j.tetlet.2007.01.122
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Ac2O; pyridine / DMAP / 12 h / 20 °C
1.2: TfOH / CH2Cl2 / 7 h / 0 - 20 °C
1.3: MeONa / methanol / 3 h / 20 °C
2.1: 93 percent / I2; PPh3; imidazole / tetrahydrofuran / 2 h / 65 °C
3.1: 98 percent / Bu3SnH; AIBN / toluene / 1 h / 110 °C
4.1: Bu2SnO / toluene; tetrahydrofuran / 2 h / Heating
4.2: Bu4NBr / toluene / 12 h / 65 °C
4.3: pyridine / 12 h / 0 - 20 °C
With
pyridine; 1H-imidazole; 2,2'-azobis(isobutyronitrile); iodine; tri-n-butyl-tin hydride; acetic anhydride; di(n-butyl)tin oxide; triphenylphosphine;
dmap;
In
tetrahydrofuran; toluene;
DOI:10.1016/j.tetlet.2007.01.122
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: Ac2O; pyridine / DMAP / 12 h / 20 °C
1.2: TfOH / CH2Cl2 / 7 h / 0 - 20 °C
1.3: MeONa / methanol / 3 h / 20 °C
2.1: 93 percent / I2; PPh3; imidazole / tetrahydrofuran / 2 h / 65 °C
3.1: 98 percent / Bu3SnH; AIBN / toluene / 1 h / 110 °C
4.1: Bu2SnO / toluene; tetrahydrofuran / 2 h / Heating
4.2: Bu4NBr / toluene / 12 h / 65 °C
4.3: pyridine / 12 h / 0 - 20 °C
With
pyridine; 1H-imidazole; 2,2'-azobis(isobutyronitrile); iodine; tri-n-butyl-tin hydride; acetic anhydride; di(n-butyl)tin oxide; triphenylphosphine;
dmap;
In
tetrahydrofuran; toluene;
DOI:10.1016/j.tetlet.2007.01.122
