N-[(2R)-2-(ethoxycarbonyl)ethyl]-N'-[(2'S)-2'-(methoxycarbonyl)phenethyl]sulfamide

Base Information

• Chemical Name: N-[(2R)-2-(ethoxycarbonyl)ethyl]-N'-[(2'S)-2'-(methoxycarbonyl)phenethyl]sulfamide
• CAS No.: 249538-94-1
• Molecular Formula: C₁₅H₂₂N₂O₆S
• Molecular Weight: 358.415

Synonyms:N-[(2R)-2-(ethoxycarbonyl)ethyl]-N'-[(2'S)-2'-(methoxycarbonyl)phenethyl]sulfamide

Chemical Property of N-[(2R)-2-(ethoxycarbonyl)ethyl]-N'-[(2'S)-2'-(methoxycarbonyl)phenethyl]sulfamide

Chemical Property:

Purity/Quality:

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Technology Process of N-[(2R)-2-(ethoxycarbonyl)ethyl]-N'-[(2'S)-2'-(methoxycarbonyl)phenethyl]sulfamide

There total 2 articles about N-[(2R)-2-(ethoxycarbonyl)ethyl]-N'-[(2'S)-2'-(methoxycarbonyl)phenethyl]sulfamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C20H30N2O8S (1026261-62-0) → N-[(2R)-2-(ethoxycarbonyl)ethyl]-N'-[(2'S)-2'-(methoxycarbonyl)phenethyl]sulfamide (249538-94-1)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

Reference yield:

<(S)(+)> methyl -phenylalaninate (139059-69-1) → N-[(2R)-2-(ethoxycarbonyl)ethyl]-N'-[(2'S)-2'-(methoxycarbonyl)phenethyl]sulfamide (249538-94-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Ph₃P; diisopropyl diazodicarboxylate / tetrahydrofuran

2: 100 percent / trifluoroacetic acid / CH₂Cl₂

With di-isopropyl azodicarboxylate; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; 1: Alkylation / 2: Hydrolysis;

Reference yield: 15.0%

methanol (67-56-1) + N-[(2R)-2-(ethoxycarbonyl)ethyl]-N'-[(2'S)-2'-(methoxycarbonyl)phenethyl]sulfamide (249538-94-1) → (4R)-[2-(methoxycarbonyl)-1-phenylethyl]-4-methyl-3-oxo-1,2,5-thiadiazolidine 1,1-dioxide + (2R,4S)-2-[2-(methoxycarbonyl)ethyl]-4-benzyl-3-oxo-1,2,5-thiadiazolidine 1,1-dioxide + (2S,4S)-2-[4-benzyl-2-(methoxycarbonyl)ethyl]-3-oxo-1,2,5-thiadiazolidine 1,1-dioxide + methoxysulfonyl-L-Phe-DL-Ala-OMe

Guidance literature:

With sodium methylate; Heating;

upstream raw materials:

C₂₀H₃₀N₂O₈S

<(S)(+)> methyl -phenylalaninate

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